N-benzoyl-4-tertbutylphenyl sulfonimidoyl fluoride

Base Information

Chemical Name:N-benzoyl-4-tertbutylphenyl sulfonimidoyl fluoride
CAS No.:1264737-63-4
Molecular Formula:C₁₇H₁₈FNO₂S
Molecular Weight:319.4
Hs Code.:

Synonyms:N-benzoyl-4-tertbutylphenyl sulfonimidoyl fluoride

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Chemical Property of N-benzoyl-4-tertbutylphenyl sulfonimidoyl fluoride

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Technology Process of N-benzoyl-4-tertbutylphenyl sulfonimidoyl fluoride

There total 6 articles about N-benzoyl-4-tertbutylphenyl sulfonimidoyl fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₇H₁₈ClNO₂S

: 1264737-63-4
N-benzoyl-4-tertbutylphenyl sulfonimidoyl fluoride

Guidance literature:: With potassium fluoride; 18-crown-6 ether; In acetonitrile; at 21 ℃; for 16h; Inert atmosphere;
DOI:10.1021/ol103030w

Reference yield:

: 1264737-41-8
4-tert-butylbenzenesulfinic acid methyl ester

: 1264737-63-4
N-benzoyl-4-tertbutylphenyl sulfonimidoyl fluoride

Guidance literature:: Multi-step reaction with 4 steps

1: lithium hexamethyldisilazane / tetrahydrofuran

2: n-butyllithium / hexane

3: tert-butylhypochlorite / dichloromethane / 2 h / 0 °C / Inert atmosphere

4: potassium fluoride; 18-crown-6 ether / acetonitrile / 16 h / 21 °C / Inert atmosphere

With potassium fluoride; n-butyllithium; 18-crown-6 ether; tert-butylhypochlorite; lithium hexamethyldisilazane; In tetrahydrofuran; hexane; dichloromethane; acetonitrile;
DOI:10.1021/ol103030w

Reference yield:

: 7605-48-3
bis(4-tert-butylphenyl)disulfide

: 1264737-63-4
N-benzoyl-4-tertbutylphenyl sulfonimidoyl fluoride

Guidance literature:: Multi-step reaction with 5 steps

1: N-Bromosuccinimide

2: lithium hexamethyldisilazane / tetrahydrofuran

3: n-butyllithium / hexane

4: tert-butylhypochlorite / dichloromethane / 2 h / 0 °C / Inert atmosphere

5: potassium fluoride; 18-crown-6 ether / acetonitrile / 16 h / 21 °C / Inert atmosphere

With potassium fluoride; N-Bromosuccinimide; n-butyllithium; 18-crown-6 ether; tert-butylhypochlorite; lithium hexamethyldisilazane; In tetrahydrofuran; hexane; dichloromethane; acetonitrile;
DOI:10.1021/ol103030w