benzyl 3-azido-2,3,6-trideoxy-4-O-methanesulfonyl-α-L-erythro-hex-2-enopyranoside

Base Information

Chemical Name:benzyl 3-azido-2,3,6-trideoxy-4-O-methanesulfonyl-α-L-erythro-hex-2-enopyranoside
CAS No.:97389-95-2
Molecular Formula:C₁₄H₁₇N₃O₅S
Molecular Weight:339.372
Hs Code.:

Synonyms:benzyl 3-azido-2,3,6-trideoxy-4-O-methanesulfonyl-α-L-erythro-hex-2-enopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 3-azido-2,3,6-trideoxy-4-O-methanesulfonyl-α-L-erythro-hex-2-enopyranoside

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Technology Process of benzyl 3-azido-2,3,6-trideoxy-4-O-methanesulfonyl-α-L-erythro-hex-2-enopyranoside

There total 4 articles about benzyl 3-azido-2,3,6-trideoxy-4-O-methanesulfonyl-α-L-erythro-hex-2-enopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 124-63-0
methanesulfonyl chloride

: 97389-93-0
benzyl 3-azido-2,3,6-trideoxy-α-L-erythro-hex-2-enopyranoside

: 97389-95-2
benzyl 3-azido-2,3,6-trideoxy-4-O-methanesulfonyl-α-L-erythro-hex-2-enopyranoside

Guidance literature:: In pyridine; at 0 - 5 ℃;
DOI:10.1016/0008-6215(85)85206-X

Reference yield:

: (2S,6R)-4-Azido-6-benzyloxy-2-methyl-3,6-dihydro-2H-pyran-3-ol

: 97389-95-2
benzyl 3-azido-2,3,6-trideoxy-4-O-methanesulfonyl-α-L-erythro-hex-2-enopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: pyridinium dichromate, molecular sieves 4 Angstroem / CH₂Cl₂ / 12 h / Ambient temperature

2: 54 percent / NaBH₄ / ethanol / Ambient temperature

3: 84 percent / pyridine / 0 - 5 °C

With sodium tetrahydroborate; dipyridinium dichromate; 4 A molecular sieve; In pyridine; ethanol; dichloromethane;
DOI:10.1016/0008-6215(85)85206-X

Reference yield:

: benzyl 4-O-acetyl-3-azido-2,3,6-trideoxy-2-iodo-α-L-altro- and mannopyranoside

: 97389-95-2
benzyl 3-azido-2,3,6-trideoxy-4-O-methanesulfonyl-α-L-erythro-hex-2-enopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: MeONa / methanol

2: pyridinium dichromate, molecular sieves 4 Angstroem / CH₂Cl₂ / 12 h / Ambient temperature

3: 54 percent / NaBH₄ / ethanol / Ambient temperature

4: 84 percent / pyridine / 0 - 5 °C

With sodium tetrahydroborate; dipyridinium dichromate; 4 A molecular sieve; sodium methylate; In pyridine; methanol; ethanol; dichloromethane;
DOI:10.1016/0008-6215(85)85206-X