(E)-3-(4-hydroxy-3-methoxyphenyl)-N'-((E)-3-(4-hydroxy-3-methoxyphenyl)acryloyl)-N,N'-diphenethylacrylohydrazide

Base Information

Chemical Name:(E)-3-(4-hydroxy-3-methoxyphenyl)-N'-((E)-3-(4-hydroxy-3-methoxyphenyl)acryloyl)-N,N'-diphenethylacrylohydrazide
CAS No.:1453190-45-8
Molecular Formula:C₃₆H₃₆N₂O₆
Molecular Weight:592.692
Hs Code.:

Synonyms:(E)-3-(4-hydroxy-3-methoxyphenyl)-N'-((E)-3-(4-hydroxy-3-methoxyphenyl)acryloyl)-N,N'-diphenethylacrylohydrazide

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Chemical Property of (E)-3-(4-hydroxy-3-methoxyphenyl)-N'-((E)-3-(4-hydroxy-3-methoxyphenyl)acryloyl)-N,N'-diphenethylacrylohydrazide

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Technology Process of (E)-3-(4-hydroxy-3-methoxyphenyl)-N'-((E)-3-(4-hydroxy-3-methoxyphenyl)acryloyl)-N,N'-diphenethylacrylohydrazide

There total 4 articles about (E)-3-(4-hydroxy-3-methoxyphenyl)-N'-((E)-3-(4-hydroxy-3-methoxyphenyl)acryloyl)-N,N'-diphenethylacrylohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₀H₄₀N₂O₈

: 1453190-45-8
(E)-3-(4-hydroxy-3-methoxyphenyl)-N'-((E)-3-(4-hydroxy-3-methoxyphenyl)acryloyl)-N,N'-diphenethylacrylohydrazide

Guidance literature:: With methanol; sodium methylate; for 1h; Reflux;
DOI:10.1016/j.tetlet.2013.07.134

Reference yield:

: 2596-47-6,147677-05-2,34749-55-8
(E)-3-(4-acetoxy-3-methoxyphenyl)acrylic acid

: 1453190-45-8
(E)-3-(4-hydroxy-3-methoxyphenyl)-N'-((E)-3-(4-hydroxy-3-methoxyphenyl)acryloyl)-N,N'-diphenethylacrylohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / Reflux; Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 1.5 h / 0 - 20 °C

3: sodium methylate; methanol / 1 h / Reflux

With methanol; thionyl chloride; sodium methylate; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1016/j.tetlet.2013.07.134

Reference yield:

: 103-63-9
1-phenyl-2-bromoethane

: 1453190-45-8
(E)-3-(4-hydroxy-3-methoxyphenyl)-N'-((E)-3-(4-hydroxy-3-methoxyphenyl)acryloyl)-N,N'-diphenethylacrylohydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydride / N,N-dimethyl-formamide / 2.5 h / 0 - 20 °C / Cooling with ice; Inert atmosphere

2: acetyl chloride; methanol / 18 h / 0 - 20 °C / Cooling with ice

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 1.5 h / 0 - 20 °C

4: sodium methylate; methanol / 1 h / Reflux

With methanol; sodium methylate; sodium hydride; N-ethyl-N,N-diisopropylamine; acetyl chloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2013.07.134