methyl 5--2,4-dinitrobenzoate

Base Information

Chemical Name:methyl 5--2,4-dinitrobenzoate
CAS No.:156423-07-3
Molecular Formula:C₁₂H₁₄ClN₃O₆
Molecular Weight:331.713
Hs Code.:

methyl 5-<N-(2-chloroethyl)-N-ethylamino>-2,4-dinitrobenzoate

Synonyms:methyl 5--2,4-dinitrobenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 5--2,4-dinitrobenzoate

Chemical Property:

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Technology Process of methyl 5--2,4-dinitrobenzoate

There total 3 articles about methyl 5--2,4-dinitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1027283-98-2
5-[Ethyl-(2-methanesulfonyloxy-ethyl)-amino]-2,4-dinitro-benzoic acid methyl ester

: 156423-07-3
methyl 5--2,4-dinitrobenzoate

Guidance literature:: With lithium chloride; In N,N-dimethyl-formamide; at 80 ℃; for 0.25h; Yield given;
DOI:10.1021/jm00040a009

Reference yield:

: 150272-08-5
methyl 5-chloro-2,4-dinitrobenzoate

: 156423-07-3
methyl 5--2,4-dinitrobenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / dioxane / 8 h / 20 °C

2: Et₃N / CH₂Cl₂ / 0.5 h / 20 °C

3: LiCl / dimethylformamide / 0.25 h / 80 °C

With triethylamine; lithium chloride; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00040a009

Reference yield:

: 156423-06-2
methyl 2,4-dinitro-5-benzoate

: 156423-07-3
methyl 5--2,4-dinitrobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 0.5 h / 20 °C

2: LiCl / dimethylformamide / 0.25 h / 80 °C

With triethylamine; lithium chloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00040a009