4,10-dimethyl-2,12-diphenyl-1,5,9,13-nitrobenzotetraazacyclo[15]tetradecinato nickel(II)

Base Information

Chemical Name:4,10-dimethyl-2,12-diphenyl-1,5,9,13-nitrobenzotetraazacyclo[15]tetradecinato nickel(II)
CAS No.:1431461-19-6
Molecular Formula:C₂₉H₂₇N₅NiO₂
Molecular Weight:536.256
Hs Code.:

Synonyms:4,10-dimethyl-2,12-diphenyl-1,5,9,13-nitrobenzotetraazacyclo[15]tetradecinato nickel(II)

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Chemical Property of 4,10-dimethyl-2,12-diphenyl-1,5,9,13-nitrobenzotetraazacyclo[15]tetradecinato nickel(II)

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Technology Process of 4,10-dimethyl-2,12-diphenyl-1,5,9,13-nitrobenzotetraazacyclo[15]tetradecinato nickel(II)

There total 1 articles about 4,10-dimethyl-2,12-diphenyl-1,5,9,13-nitrobenzotetraazacyclo[15]tetradecinato nickel(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: Ni(1-phenylbutanedione-1,3)2

: C₂₆H₂₁N₃NiO₄

: 6018-89-9
nickel(II) acetate tetrahydrate

: 109-76-2,54018-94-9
Trimethylenediamine

: 99-56-9
4-Nitrophenylene-1,2-diamine

: 93-91-4
1-phenylbutan-1,3-dione

: 1431461-19-6
4,10-dimethyl-2,12-diphenyl-1,5,9,13-nitrobenzotetraazacyclo[15]tetradecinato nickel(II)

Guidance literature:: nickel(II) acetate tetrahydrate; 1-phenylbutan-1,3-dione; In ethanol; for 0.333333h; Reflux;

Ni(1-phenylbutanedione-1,3)2; 4-Nitrophenylene-1,2-diamine; In ethanol; for 0.0833333h;

C₂₆H₂₁N₃NiO₄; Trimethylenediamine; In ethanol; for 12h; Inert atmosphere; Reflux;
DOI:10.1016/j.ica.2012.12.041