ethyl 3-(benzyloxy)-4-(3-(4-methoxytetrahydro-2H-pyran-4-yl)benzyloxy)benzoate

Base Information

Chemical Name:ethyl 3-(benzyloxy)-4-(3-(4-methoxytetrahydro-2H-pyran-4-yl)benzyloxy)benzoate
CAS No.:1289486-16-3
Molecular Formula:C₂₉H₃₂O₆
Molecular Weight:476.569
Hs Code.:

Synonyms:ethyl 3-(benzyloxy)-4-(3-(4-methoxytetrahydro-2H-pyran-4-yl)benzyloxy)benzoate

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Chemical Property of ethyl 3-(benzyloxy)-4-(3-(4-methoxytetrahydro-2H-pyran-4-yl)benzyloxy)benzoate

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Technology Process of ethyl 3-(benzyloxy)-4-(3-(4-methoxytetrahydro-2H-pyran-4-yl)benzyloxy)benzoate

There total 7 articles about ethyl 3-(benzyloxy)-4-(3-(4-methoxytetrahydro-2H-pyran-4-yl)benzyloxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 188564-63-8
ethyl 4-hydroxy-3-(phenylmethoxy)benzoate

: 144800-91-9
4-(3-(bromomethyl)phenyl)-4-methoxytetrahydro-2H-pyran

: 1289486-16-3
ethyl 3-(benzyloxy)-4-(3-(4-methoxytetrahydro-2H-pyran-4-yl)benzyloxy)benzoate

Guidance literature:: With potassium carbonate; In acetone; Reflux;
DOI:10.1016/j.bmc.2011.01.043

Reference yield:

: 29943-42-8,143562-54-3
Tetrahydro-4H-pyran-4-one

: 1289486-16-3
ethyl 3-(benzyloxy)-4-(3-(4-methoxytetrahydro-2H-pyran-4-yl)benzyloxy)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: magnesium / tetrahydrofuran / Reflux

1.2: 1 h / Reflux

2.1: sodium hydride / tetrahydrofuran; mineral oil / 15 h / 20 °C

3.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 1.5 h / Reflux

4.1: potassium carbonate / acetone / Reflux

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); sodium hydride; potassium carbonate; magnesium; In tetrahydrofuran; tetrachloromethane; acetone; mineral oil;
DOI:10.1016/j.bmc.2011.01.043

Reference yield:

: 99-50-3
3,4-Dihydroxybenzoic acid

: 1289486-16-3
ethyl 3-(benzyloxy)-4-(3-(4-methoxytetrahydro-2H-pyran-4-yl)benzyloxy)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid / 3 h / 50 °C

2: potassium carbonate / acetone / 3 h / Reflux

3: potassium carbonate / acetone / Reflux

With sulfuric acid; potassium carbonate; In acetone;
DOI:10.1016/j.bmc.2011.01.043