3-chloromercuri-1-(p-cresoxy)-2,3,3a,8b-tetrahydro-1H-cyclopentabenzofuran

Base Information

• Chemical Name: 3-chloromercuri-1-(p-cresoxy)-2,3,3a,8b-tetrahydro-1H-cyclopentabenzofuran
• CAS No.: 106550-35-0
• Molecular Formula: C₁₉H₁₉ClHgO₂
• Molecular Weight: 515.402

Synonyms:3-chloromercuri-1-(p-cresoxy)-2,3,3a,8b-tetrahydro-1H-cyclopentabenzofuran

Chemical Property of 3-chloromercuri-1-(p-cresoxy)-2,3,3a,8b-tetrahydro-1H-cyclopentabenzofuran

Chemical Property:

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Technology Process of 3-chloromercuri-1-(p-cresoxy)-2,3,3a,8b-tetrahydro-1H-cyclopentabenzofuran

There total 2 articles about 3-chloromercuri-1-(p-cresoxy)-2,3,3a,8b-tetrahydro-1H-cyclopentabenzofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-cresol (106-44-5) → 3-chloromercuri-1-(p-cresoxy)-2,3,3a,8b-tetrahydro-1H-cyclopentabenzofuran (106550-35-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) KOH / 1.) 90percent ethanol, reflux, 1 h, 2.) 6 h

2: 62 percent / N,N-diethylaniline / 10 h / Heating

3: 65 percent / HgCl₂ / H₂O / 24 h / Ambient temperature

With potassium hydroxide; N,N-diethylaniline; mercury dichloride; In water;

Reference yield:

trans-3,5-bis-p-cresoxycyclopentene (106550-27-0) → 3-chloromercuri-1-(p-cresoxy)-2,3,3a,8b-tetrahydro-1H-cyclopentabenzofuran (106550-35-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 62 percent / N,N-diethylaniline / 10 h / Heating

2: 65 percent / HgCl₂ / H₂O / 24 h / Ambient temperature

With N,N-diethylaniline; mercury dichloride; In water;

Reference yield: 80.0%

3-chloromercuri-1-(p-cresoxy)-2,3,3a,8b-tetrahydro-1H-cyclopentabenzofuran (106550-35-0) → 3-bromo-1-(p-cresoxy)-2,3,3a,8b-tetrahydro-1H-cyclopentabenzofuran (106550-36-1)

Guidance literature:

With bromine; In chloroform; at 50 ℃; for 0.75h; Irradiation;

upstream raw materials:

p-cresol

trans-3,5-bis-p-cresoxycyclopentene

Downstream raw materials:

3-bromo-1-(p-cresoxy)-2,3,3a,8b-tetrahydro-1H-cyclopentabenzofuran

7-Methyl-1-p-tolyloxy-3a,8b-dihydro-1H-benzo[b]cyclopenta[d]furan

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