O-ethyl S-[1-(N-acetyl-N-(4-methoxybenzenesulfonyl)aminomethyl)-3-cyanopropyl] dithiocarbonate

Base Information

Chemical Name:O-ethyl S-[1-(N-acetyl-N-(4-methoxybenzenesulfonyl)aminomethyl)-3-cyanopropyl] dithiocarbonate
CAS No.:946076-30-8
Molecular Formula:C₁₇H₂₂N₂O₅S₃
Molecular Weight:430.57
Hs Code.:

Synonyms:O-ethyl S-[1-(N-acetyl-N-(4-methoxybenzenesulfonyl)aminomethyl)-3-cyanopropyl] dithiocarbonate

Suppliers and Price of O-ethyl S-[1-(N-acetyl-N-(4-methoxybenzenesulfonyl)aminomethyl)-3-cyanopropyl] dithiocarbonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-ethyl S-[1-(N-acetyl-N-(4-methoxybenzenesulfonyl)aminomethyl)-3-cyanopropyl] dithiocarbonate

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Technology Process of O-ethyl S-[1-(N-acetyl-N-(4-methoxybenzenesulfonyl)aminomethyl)-3-cyanopropyl] dithiocarbonate

There total 2 articles about O-ethyl S-[1-(N-acetyl-N-(4-methoxybenzenesulfonyl)aminomethyl)-3-cyanopropyl] dithiocarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34954-40-0
N-allyl-4-methoxybenzenesulfonamide

: 946076-30-8
O-ethyl S-[1-(N-acetyl-N-(4-methoxybenzenesulfonyl)aminomethyl)-3-cyanopropyl] dithiocarbonate

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / toluene / 48 h / Heating

2: 58 percent / lauroyl peroxide / 1,2-dichloro-ethane / Heating

With dilauryl peroxide; In 1,2-dichloro-ethane; toluene;
DOI:10.1016/j.tet.2007.04.091

Reference yield:

: 98-68-0
4-methoxy-phenyl-sulphonyl chloride

: 946076-30-8
O-ethyl S-[1-(N-acetyl-N-(4-methoxybenzenesulfonyl)aminomethyl)-3-cyanopropyl] dithiocarbonate

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / NaOH / H₂O; diethyl ether / 5 h / 20 °C

2: 84 percent / toluene / 48 h / Heating

3: 58 percent / lauroyl peroxide / 1,2-dichloro-ethane / Heating

With sodium hydroxide; dilauryl peroxide; In diethyl ether; water; 1,2-dichloro-ethane; toluene; 1: Schotten-Baumann reaction;
DOI:10.1016/j.tet.2007.04.091