3-Bromo-1-(2,4-dichlorophenyl)-4-(4-heptylamino)-6-methyl-5,7-diazaindole

Base Information

Chemical Name:3-Bromo-1-(2,4-dichlorophenyl)-4-(4-heptylamino)-6-methyl-5,7-diazaindole
CAS No.:268547-65-5
Molecular Formula:C₂₀H₂₃BrCl₂N₄
Molecular Weight:470.239
Hs Code.:

Synonyms:3-Bromo-1-(2,4-dichlorophenyl)-4-(4-heptylamino)-6-methyl-5,7-diazaindole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Bromo-1-(2,4-dichlorophenyl)-4-(4-heptylamino)-6-methyl-5,7-diazaindole

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Technology Process of 3-Bromo-1-(2,4-dichlorophenyl)-4-(4-heptylamino)-6-methyl-5,7-diazaindole

There total 5 articles about 3-Bromo-1-(2,4-dichlorophenyl)-4-(4-heptylamino)-6-methyl-5,7-diazaindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 16751-59-0
4-heptylamine

: 644994-55-8
5-bromo-4-chloro-7-(2,4-dichloro-phenyl)-2-methyl-7H-pyrrolo[2,3-d]pyrimidine

: 268547-65-5
3-Bromo-1-(2,4-dichlorophenyl)-4-(4-heptylamino)-6-methyl-5,7-diazaindole

Guidance literature:: With toluene-4-sulfonic acid; at 90 ℃;
DOI:10.3987/COM-03-S(P)41

Reference yield:

: 95-14-7,27556-51-0
1,2,3-Benzotriazole

: 16751-59-0
4-heptylamine

: 268547-65-5
3-Bromo-1-(2,4-dichlorophenyl)-4-(4-heptylamino)-6-methyl-5,7-diazaindole

Guidance literature:: With bromine; In 1,4-dioxane;

Reference yield:

: 85826-33-1
5-Allyl-2-methyl-4,6-dichloropyrimidine

: 268547-65-5
3-Bromo-1-(2,4-dichlorophenyl)-4-(4-heptylamino)-6-methyl-5,7-diazaindole

Guidance literature:: Multi-step reaction with 4 steps

1.1: 37 percent / NaH / dimethylformamide

2.1: osmium tetroxide; sodium periodate / acetone; H₂O

2.2: 53 percent / aq. HCl / CH₂Cl₂

3.1: 100 percent / Br₂ / dioxane

4.1: 70 percent / TsOH / 90 °C

With sodium periodate; osmium(VIII) oxide; bromine; sodium hydride; toluene-4-sulfonic acid; In 1,4-dioxane; water; N,N-dimethyl-formamide; acetone;
DOI:10.3987/COM-03-S(P)41