3-isopropoxy-4-(3-isopropoxy-4-(3-isopropoxy-4-amino-benzoylamido)-benzoylamido)-benzoic acid

Base Information

Chemical Name:3-isopropoxy-4-(3-isopropoxy-4-(3-isopropoxy-4-amino-benzoylamido)-benzoylamido)-benzoic acid
CAS No.:1190360-14-5
Molecular Formula:C₃₀H₃₅N₃O₇
Molecular Weight:549.624
Hs Code.:

Synonyms:3-isopropoxy-4-(3-isopropoxy-4-(3-isopropoxy-4-amino-benzoylamido)-benzoylamido)-benzoic acid

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Chemical Property of 3-isopropoxy-4-(3-isopropoxy-4-(3-isopropoxy-4-amino-benzoylamido)-benzoylamido)-benzoic acid

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Technology Process of 3-isopropoxy-4-(3-isopropoxy-4-(3-isopropoxy-4-amino-benzoylamido)-benzoylamido)-benzoic acid

There total 9 articles about 3-isopropoxy-4-(3-isopropoxy-4-(3-isopropoxy-4-amino-benzoylamido)-benzoylamido)-benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1006031-03-3
methyl 3-isopropoxy-4-(3-isopropoxy-4-(3-isopropoxy-4-amino-benzoylamino)-benzoylamino)-benzoate

: 1190360-14-5
3-isopropoxy-4-(3-isopropoxy-4-(3-isopropoxy-4-amino-benzoylamido)-benzoylamido)-benzoic acid

Guidance literature:: With water; sodium hydroxide; In tetrahydrofuran; methanol;
DOI:10.1039/b908207g

Reference yield:

: 159783-41-2
methyl 3-isopropyloxy-4-nitrobenzoate

: 1190360-14-5
3-isopropoxy-4-(3-isopropoxy-4-(3-isopropoxy-4-amino-benzoylamido)-benzoylamido)-benzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: lithium hydroxide monohydrate / tetrahydrofuran; methanol; water / 1 h / 20 °C / Inert atmosphere

2: dichlorotriphenylphosphorane / chloroform / Reflux; Inert atmosphere

3: tin(II) chloride dihdyrate / ethyl acetate / 12 h / 50 °C / Inert atmosphere

4: water; sodium hydroxide / tetrahydrofuran; methanol / 20 °C / Inert atmosphere

With tin(II) chloride dihdyrate; lithium hydroxide monohydrate; water; sodium hydroxide; dichlorotriphenylphosphorane; In tetrahydrofuran; methanol; chloroform; water; ethyl acetate;
DOI:10.1039/c2ob07125h

Reference yield:

: 619-14-7
3-hydroxy-4-nitro-benzoic acid

: 1190360-14-5
3-isopropoxy-4-(3-isopropoxy-4-(3-isopropoxy-4-amino-benzoylamido)-benzoylamido)-benzoic acid

Guidance literature:: Multi-step reaction with 6 steps

1.1: thionyl chloride / 12 h / 0 °C / Reflux; Inert atmosphere

2.1: triphenylphosphine / tetrahydrofuran / 0.03 h / 20 °C / Inert atmosphere

2.2: 16 h / Inert atmosphere

3.1: lithium hydroxide monohydrate / tetrahydrofuran; methanol; water / 1 h / 20 °C / Inert atmosphere

4.1: dichlorotriphenylphosphorane / chloroform / Reflux; Inert atmosphere

5.1: tin(II) chloride dihdyrate / ethyl acetate / 12 h / 50 °C / Inert atmosphere

6.1: water; sodium hydroxide / tetrahydrofuran; methanol / 20 °C / Inert atmosphere

With thionyl chloride; tin(II) chloride dihdyrate; lithium hydroxide monohydrate; water; triphenylphosphine; sodium hydroxide; dichlorotriphenylphosphorane; In tetrahydrofuran; methanol; chloroform; water; ethyl acetate;
DOI:10.1039/c2ob07125h