C₂₅H₂₆NO₆P

Base Information

Chemical Name:C₂₅H₂₆NO₆P
CAS No.:1393365-85-9
Molecular Formula:C₂₅H₂₆NO₆P
Molecular Weight:467.458
Hs Code.:

C<sub>25</sub>H<sub>26</sub>NO<sub>6</sub>P

Synonyms:C₂₅H₂₆NO₆P

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Chemical Property of C₂₅H₂₆NO₆P

Chemical Property:

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Technology Process of C₂₅H₂₆NO₆P

There total 3 articles about C₂₅H₂₆NO₆P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1-methyl-3-iodo-indole-2-carboxylic acid

: 1078138-44-9
C₁₅H₁₉O₄P

: 1393365-85-9
C₂₅H₂₆NO₆P

Guidance literature:: With palladium diacetate; cesium fluoride; tris-(o-tolyl)phosphine; In N,N-dimethyl-formamide; at 80 ℃; for 14h; regioselective reaction;
DOI:10.1021/jo301149s

Reference yield:

: ethyl 1-methyl-3-iodoindole-2-carboxylate

: 1393365-85-9
C₂₅H₂₆NO₆P

Guidance literature:: Multi-step reaction with 2 steps

1: water; potassium hydroxide / ethanol / 16 h / Reflux

2: palladium diacetate; cesium fluoride; tris-(o-tolyl)phosphine / N,N-dimethyl-formamide / 14 h / 80 °C

With water; palladium diacetate; cesium fluoride; tris-(o-tolyl)phosphine; potassium hydroxide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jo301149s

Reference yield:

: 117637-79-3
ethyl 3-iodo-1H-indole-2-carboxylate

: 1393365-85-9
C₂₅H₂₆NO₆P

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutylammomium bromide; potassium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C

2: water; potassium hydroxide / ethanol / 16 h / Reflux

3: palladium diacetate; cesium fluoride; tris-(o-tolyl)phosphine / N,N-dimethyl-formamide / 14 h / 80 °C

With tetrabutylammomium bromide; water; palladium diacetate; potassium carbonate; cesium fluoride; tris-(o-tolyl)phosphine; potassium hydroxide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jo301149s