N-[2-hydroxy-1-(4-hydroxy-3-hydroxymethylphenylcarbamoyl)ethyl] decanamide

Base Information

Chemical Name:N-[2-hydroxy-1-(4-hydroxy-3-hydroxymethylphenylcarbamoyl)ethyl] decanamide
CAS No.:282108-75-2
Molecular Formula:C₂₀H₃₂N₂O₅
Molecular Weight:380.484
Hs Code.:

Synonyms:N-[2-hydroxy-1-(4-hydroxy-3-hydroxymethylphenylcarbamoyl)ethyl] decanamide

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Chemical Property of N-[2-hydroxy-1-(4-hydroxy-3-hydroxymethylphenylcarbamoyl)ethyl] decanamide

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Technology Process of N-[2-hydroxy-1-(4-hydroxy-3-hydroxymethylphenylcarbamoyl)ethyl] decanamide

There total 7 articles about N-[2-hydroxy-1-(4-hydroxy-3-hydroxymethylphenylcarbamoyl)ethyl] decanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 104333-09-7
4-amino-2-hydroxymethylphenol

: 282108-72-9
N-Decanoyl-D-serine

: 282108-75-2
N-[2-hydroxy-1-(4-hydroxy-3-hydroxymethylphenylcarbamoyl)ethyl] decanamide

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; for 16h;
DOI:10.1002/(SICI)1521-3773(20000417)39:8<1440::AID-ANIE1440>3.0.CO;2-R

Reference yield:

: 39224-61-8
2-hydroxy-5-nitrobenzyl alcohol

: 282108-75-2
N-[2-hydroxy-1-(4-hydroxy-3-hydroxymethylphenylcarbamoyl)ethyl] decanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / H₂ / Pd-C / methanol / 5 h

2: 61 percent / DCC; HOBt / dimethylformamide / 0 - 20 °C

With hydrogen; benzotriazol-1-ol; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1002/1099-0690(200101)2001:1<137::AID-EJOC137>3.0.CO;2-#

Reference yield:

: 97-51-8
5-Nitrosalicylaldehyde

: 282108-75-2
N-[2-hydroxy-1-(4-hydroxy-3-hydroxymethylphenylcarbamoyl)ethyl] decanamide

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / NaBH₄ / ethanol

2: 97 percent / H₂ / Pd-C / methanol / 5 h

3: 61 percent / DCC; HOBt / dimethylformamide / 0 - 20 °C

With sodium tetrahydroborate; hydrogen; benzotriazol-1-ol; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1002/1099-0690(200101)2001:1<137::AID-EJOC137>3.0.CO;2-#