p-ethoxyaniline hydrobromide

Base Information

• Chemical Name: p-ethoxyaniline hydrobromide
• CAS No.: 108160-45-8
• Molecular Formula: BrH*C₈H₁₁NO
• Molecular Weight: 218.093

Synonyms:p-ethoxyaniline hydrobromide

Chemical Property of p-ethoxyaniline hydrobromide

Chemical Property:

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Technology Process of p-ethoxyaniline hydrobromide

There total 1 articles about p-ethoxyaniline hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Ethoxyaniline (156-43-4) → p-ethoxyaniline hydrobromide (108160-45-8)

Guidance literature:

With hydrogen bromide; In water; at 30 - 35 ℃; for 0.666667h; Autoclave; Large scale;

Reference yield: 94.7%

p-ethoxyaniline hydrobromide (108160-45-8) + acetic anhydride (108-24-7) → 4-ethoxyacetanilide (62-44-2,105931-34-8)

Guidance literature:

In aq. acetate buffer; at 90 - 93 ℃; for 6.5h; pH=4 - 5; Large scale;

Reference yield:

sodium hexabromo osmate(IV) + p-ethoxyaniline hydrobromide (108160-45-8) → p-phenetidinium osmium(IV) bromide

Guidance literature:

In hydrogen bromide; bromide dissolved in dild. HBr added to the soln. of Na2{OsBr6} at common temp.; excess of Os-soln.; crystalline or oily product;; crystn. of the oily product by grinding or by dissoln. in hot alcohol and cooling or evapn. of the soln.; crystn. by addn. of small amounts of HBr (with some drops of alc.) to the product in mother liquor at higher temp.;;

upstream raw materials:

4-Ethoxyaniline

Downstream raw materials:

4-ethoxyacetanilide

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