C₃₀H₄₂O₈

Base Information

Chemical Name:C₃₀H₄₂O₈
CAS No.:1419178-84-9
Molecular Formula:C₃₀H₄₂O₈
Molecular Weight:530.659
Hs Code.:

C<sub>30</sub>H<sub>42</sub>O<sub>8</sub>

Synonyms:C₃₀H₄₂O₈

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Chemical Property of C₃₀H₄₂O₈

Chemical Property:

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Technology Process of C₃₀H₄₂O₈

There total 17 articles about C₃₀H₄₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1419179-10-4
C₃₃H₄₆O₈

: 1419178-84-9
C₃₀H₄₂O₈

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; for 3h; Inert atmosphere; Reflux;
DOI:10.1021/jo302353g

Reference yield:

: 66323-03-3
4,5-bis(hydroxy)phthalic acid dimethyl ester

: 1419178-84-9
C₃₀H₄₂O₈

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetone / 6 h / Inert atmosphere; Reflux

2: caesium carbonate / acetone / 4 h / Inert atmosphere; Reflux

3: chloro-trimethyl-silane; trimethylsilyl trifluoromethanesulfonate / 1,2-dichloro-ethane / 3 h / 0 °C / Inert atmosphere; Reflux

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / ethanol / 3 h / Inert atmosphere; Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; chloro-trimethyl-silane; trimethylsilyl trifluoromethanesulfonate; potassium carbonate; caesium carbonate; In ethanol; 1,2-dichloro-ethane; acetone;
DOI:10.1021/jo302353g

Reference yield:

: 111-24-0
1,5-dibromo-pentane

: 1419178-84-9
C₃₀H₄₂O₈

Guidance literature:: Multi-step reaction with 11 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.08 h / 0 °C / Inert atmosphere

1.2: 12 h / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane; N,N,N,N,N,N-hexamethylphosphoric triamide / 0 °C / Inert atmosphere

2.2: 2 h / 0 °C / Inert atmosphere

3.1: pyridinium p-toluenesulfonate / ethanol / 0.5 h / Inert atmosphere; Reflux

4.1: sodium; ammonia / tetrahydrofuran; tert-butyl alcohol / 1 h / -40 °C / Inert atmosphere

5.1: Dess-Martin periodane / dichloromethane / 0.17 h / 20 °C / Inert atmosphere

6.1: tert.-butyl lithium / tetrahydrofuran; pentane / 1.5 h / -25 °C / Inert atmosphere

6.2: 0.33 h / -78 °C / Inert atmosphere

7.1: bis-[(trifluoroacetoxy)iodo]benzene / methanol; water / 0.08 h / Inert atmosphere

8.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 0.5 h / Inert atmosphere

9.1: caesium carbonate / acetone / 4 h / Inert atmosphere; Reflux

10.1: chloro-trimethyl-silane; trimethylsilyl trifluoromethanesulfonate / 1,2-dichloro-ethane / 3 h / 0 °C / Inert atmosphere; Reflux

11.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / ethanol / 3 h / Inert atmosphere; Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; chloro-trimethyl-silane; carbon tetrabromide; trimethylsilyl trifluoromethanesulfonate; ammonia; tert.-butyl lithium; sodium; pyridinium p-toluenesulfonate; caesium carbonate; Dess-Martin periodane; triphenylphosphine; bis-[(trifluoroacetoxy)iodo]benzene; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; hexane; dichloromethane; water; 1,2-dichloro-ethane; acetone; tert-butyl alcohol; pentane;
DOI:10.1021/jo302353g