C₄₃H₇₀O₁₀Si

Base Information

Chemical Name:C₄₃H₇₀O₁₀Si
CAS No.:1325710-87-9
Molecular Formula:C₄₃H₇₀O₁₀Si
Molecular Weight:775.108
Hs Code.:

C<sub>43</sub>H<sub>70</sub>O<sub>10</sub>Si

Synonyms:C₄₃H₇₀O₁₀Si

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Chemical Property of C₄₃H₇₀O₁₀Si

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Technology Process of C₄₃H₇₀O₁₀Si

There total 20 articles about C₄₃H₇₀O₁₀Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1325711-12-3
C₄₁H₆₆O₉Si

: 107-30-2
chloromethyl methyl ether

: 1325710-87-9
C₄₃H₇₀O₁₀Si

Guidance literature:: With dmap; N-ethyl-N,N-diisopropylamine; sodium iodide; In dichloromethane; at 0 - 20 ℃; for 12h;
DOI:10.1021/ol201920j

Reference yield:

: 913066-81-6
[(1R,3S,4R,5R,7R)-4-Methyl-3-((E)-styryl)-2,6-dioxa-bicyclo[3.2.1]oct-7-yl]-methanol

: 1325710-87-9
C₄₃H₇₀O₁₀Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere

1.2: 2 h / 0 °C / Inert atmosphere

2.1: sodium periodate; osmium(VIII) oxide / tetrahydrofuran; water / 2 h / pH 7 / Inert atmosphere; aq. buffer

3.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

3.2: 1 h / 0 °C / Inert atmosphere

4.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / toluene / 18 h / 20 °C / Inert atmosphere

5.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1.25 h / -78 - -40 °C / Inert atmosphere

5.2: 2 h / -78 - 20 °C

6.1: dimethyl zinc(II); tert.-butyl lithium / tetrahydrofuran; n-heptane; pentane / 1.75 h / -78 °C / Inert atmosphere

6.2: 3 h / -78 °C / Inert atmosphere

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 24 h / 0 - 20 °C

8.1: camphor-10-sulfonic acid / 12 h / 20 °C / Inert atmosphere

9.1: 1H-imidazole / dichloromethane / 12 h / 20 °C / Inert atmosphere

10.1: dmap; N-ethyl-N,N-diisopropylamine; sodium iodide / dichloromethane / 12 h / 0 - 20 °C

With 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; dmap; sodium periodate; osmium(VIII) oxide; oxalyl dichloride; camphor-10-sulfonic acid; potassium tert-butylate; tetrabutyl ammonium fluoride; dimethyl zinc(II); tert.-butyl lithium; sodium hydride; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; sodium iodide; In tetrahydrofuran; n-heptane; dichloromethane; water; N,N-dimethyl-formamide; toluene; mineral oil; pentane; 3.1: Wittig reaction / 3.2: Wittig reaction / 5.1: Swern oxidation / 5.2: Swern oxidation;
DOI:10.1021/ol201920j

Reference yield:

: 1325710-61-9
C₂₉H₆₂O₄Si₃

: 1325710-87-9
C₄₃H₇₀O₁₀Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / toluene / 18 h / 20 °C / Inert atmosphere

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1.25 h / -78 - -40 °C / Inert atmosphere

2.2: 2 h / -78 - 20 °C

3.1: dimethyl zinc(II); tert.-butyl lithium / tetrahydrofuran; n-heptane; pentane / 1.75 h / -78 °C / Inert atmosphere

3.2: 3 h / -78 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 24 h / 0 - 20 °C

5.1: camphor-10-sulfonic acid / 12 h / 20 °C / Inert atmosphere

6.1: 1H-imidazole / dichloromethane / 12 h / 20 °C / Inert atmosphere

7.1: dmap; N-ethyl-N,N-diisopropylamine; sodium iodide / dichloromethane / 12 h / 0 - 20 °C

With 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; dmap; oxalyl dichloride; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; dimethyl zinc(II); tert.-butyl lithium; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; sodium iodide; In tetrahydrofuran; n-heptane; dichloromethane; toluene; pentane; 2.1: Swern oxidation / 2.2: Swern oxidation;
DOI:10.1021/ol201920j