1-(3,5-Dimethyl-phenyl)-1H-[1,2,4]triazole-3,5-dicarboxylic acid dimethyl ester

Base Information

• Chemical Name: 1-(3,5-Dimethyl-phenyl)-1H-[1,2,4]triazole-3,5-dicarboxylic acid dimethyl ester
• CAS No.: 125240-47-3
• Molecular Formula: C₁₄H₁₅N₃O₄
• Molecular Weight: 289.291

Synonyms:1-(3,5-Dimethyl-phenyl)-1H-[1,2,4]triazole-3,5-dicarboxylic acid dimethyl ester

Chemical Property of 1-(3,5-Dimethyl-phenyl)-1H-[1,2,4]triazole-3,5-dicarboxylic acid dimethyl ester

Chemical Property:

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Technology Process of 1-(3,5-Dimethyl-phenyl)-1H-[1,2,4]triazole-3,5-dicarboxylic acid dimethyl ester

There total 7 articles about 1-(3,5-Dimethyl-phenyl)-1H-[1,2,4]triazole-3,5-dicarboxylic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

methyl α-aminoglyoxylate phenylhydrazone (74669-09-3) + C11H13N5O2 (125240-33-7) → 3,5-dimethylbiphenyl (17057-88-4) + 1-phenyl-1H-[1,2,4]triazole-3,5-dicarboxylic acid dimethyl ester (125240-45-1) + C11H15N3O2 (125240-38-2) + methyl 2-(3,5-dimethylphenylhydrazono)-2-phenylacetate (125240-55-3) + (3,5-Dimethyl-phenyl)-[(3,5-dimethyl-phenyl)-hydrazono]-acetic acid methyl ester (125240-43-9) + 1-(3,5-Dimethyl-phenyl)-1H-[1,2,4]triazole-3,5-dicarboxylic acid dimethyl ester (125240-47-3)

Guidance literature:

In benzene; for 5h; Product distribution; Mechanism; Heating;

Reference yield: 12.0%

C11H13N5O2 (125240-33-7) → 3,5-dimethylbiphenyl (17057-88-4) + 1-phenyl-1H-[1,2,4]triazole-3,5-dicarboxylic acid dimethyl ester (125240-45-1) + C11H15N3O2 (125240-38-2) + 1-(3,5-Dimethyl-phenyl)-1H-[1,2,4]triazole-3,5-dicarboxylic acid dimethyl ester (125240-47-3)

Guidance literature:

With methyl α-aminoglyoxylate phenylhydrazone; In benzene; for 5h; Further byproducts given; Heating;

Reference yield: 9.0%

C11H15N3O2 (125240-38-2) → 3,5-dimethylbiphenyl (17057-88-4) + 1-(3,5-Dimethyl-phenyl)-1H-[1,2,4]triazole-3,5-dicarboxylic acid dimethyl ester (125240-47-3)

Guidance literature:

With manganese(IV) oxide; In benzene; for 4h; Ambient temperature;

upstream raw materials:

methyl α-aminoglyoxylate phenylhydrazone

C₁₁H₁₃N₅O₂

C₁₁H₁₅N₃O₂

C₁₁H₁₃ClN₂O₂

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