methyl α-aminoglyoxylate phenylhydrazone

Base Information

• Chemical Name: methyl α-aminoglyoxylate phenylhydrazone
• CAS No.: 74669-09-3
• Molecular Formula: C₉H₁₁N₃O₂
• Molecular Weight: 193.205

Synonyms:methyl α-aminoglyoxylate phenylhydrazone

Chemical Property of methyl α-aminoglyoxylate phenylhydrazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of methyl α-aminoglyoxylate phenylhydrazone

There total 6 articles about methyl α-aminoglyoxylate phenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

N′-(4-fluorophenyl)benzamidine (21719-88-0) + methyl 2-chloro-2-(2-phenylhydrazono)acetate (58131-64-9) → 1,5-diphenyl-3-methoxycarbonal-1,2,4-triazole (89060-64-0) + methyl α-aminoglyoxylate phenylhydrazone (74669-09-3) + 3-(4-Fluoro-phenyl)-2-phenyl-5-(phenyl-hydrazono)-3,5-dihydro-imidazol-4-one (74669-00-4) + 4-fluoroaniline (371-40-4)

Guidance literature:

With triethylamine; In chloroform; for 4h; Further byproducts given;

Reference yield: 23.0%

Methyl azido-(phenylhydrazono)-acetate (93831-03-9) → methyl 2-oxo-2-phenylacetate (15206-55-0) + methyl 1-phenyl-1H-1,2,4-triazole-3-carboxylate (57226-96-7) + 1-phenyl-1H-[1,2,4]triazole-3,5-dicarboxylic acid dimethyl ester (125240-45-1) + methyl α-aminoglyoxylate phenylhydrazone (74669-09-3)

Guidance literature:

In 1,4-dioxane; for 2h; Further byproducts given; Heating; benzene, 4 h;

Reference yield: 15.0%

Methyl azido-(phenylhydrazono)-acetate (93831-03-9) → biphenyl (92-52-4,1594-86-1) + 1-phenyl-1H-[1,2,4]triazole-3,5-dicarboxylic acid dimethyl ester (125240-45-1) + methyl α-aminoglyoxylate phenylhydrazone (74669-09-3) + methyl benzoyl formate phenylhydrazone (23102-13-8)

Guidance literature:

In benzene; for 4h; Heating;

upstream raw materials:

Methyl azido-(phenylhydrazono)-acetate

N′-(4-fluorophenyl)benzamidine

methyl 2-chloro-2-(2-phenylhydrazono)acetate

Downstream raw materials:

3,5-dimethylbiphenyl

1-phenyl-1H-[1,2,4]triazole-3,5-dicarboxylic acid dimethyl ester

C₁₁H₁₅N₃O₂

methyl 2-(3,5-dimethylphenylhydrazono)-2-phenylacetate

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 74669-09-3 methyl α-aminoglyoxylate phenylhydrazone

Send

Send

Metric Ton KG G Pound L ML

Send

Send