1-<5-O-tert-butyldiphenylsilyl)-2,3-dideoxy-2-phenylthio-α-D-erythro-pentofuranosyl>uracil

Base Information

Chemical Name:1-<5-O-tert-butyldiphenylsilyl)-2,3-dideoxy-2-phenylthio-α-D-erythro-pentofuranosyl>uracil
CAS No.:132336-17-5
Molecular Formula:C₃₁H₃₄N₂O₄SSi
Molecular Weight:558.773
Hs Code.:

Synonyms:1-<5-O-tert-butyldiphenylsilyl)-2,3-dideoxy-2-phenylthio-α-D-erythro-pentofuranosyl>uracil

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Chemical Property of 1-<5-O-tert-butyldiphenylsilyl)-2,3-dideoxy-2-phenylthio-α-D-erythro-pentofuranosyl>uracil

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Technology Process of 1-<5-O-tert-butyldiphenylsilyl)-2,3-dideoxy-2-phenylthio-α-D-erythro-pentofuranosyl>uracil

There total 2 articles about 1-<5-O-tert-butyldiphenylsilyl)-2,3-dideoxy-2-phenylthio-α-D-erythro-pentofuranosyl>uracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 132436-48-7
1-O-acetyl-5-O-(tert-butyldiphenylsilyl)-2,3-dideoxy-2-phenylthio-D-erythro-pentofuranose

: 10457-14-4
O,O'-bis-(trimethylsilyl)uracil

: 132336-17-5
1-<5-O-tert-butyldiphenylsilyl)-2,3-dideoxy-2-phenylthio-α-D-erythro-pentofuranosyl>uracil

: 132343-22-7
1-<5-O-(tert-butyldiphenylsilyl)-2,3-dideoxy-2-phenylthio-β-D-erythro-pentofuranosyl>uracil

Guidance literature:: tin(IV) chloride; In 1,2-dichloro-ethane; at 0 ℃; for 3.5h; Title compound not separated from byproducts;
DOI:10.1246/cl.1990.1459

Reference yield:

: 149204-36-4
(1S)-1-<<(tert-butyldiphenylsilyl)oxy>methyl>-2,3-dihydrofuran

: 931-59-9
benzenesulfenyl chloride

: 10457-14-4
O,O'-bis-(trimethylsilyl)uracil

: 132336-17-5
1-<5-O-tert-butyldiphenylsilyl)-2,3-dideoxy-2-phenylthio-α-D-erythro-pentofuranosyl>uracil

: 132343-22-7
1-<5-O-(tert-butyldiphenylsilyl)-2,3-dideoxy-2-phenylthio-β-D-erythro-pentofuranosyl>uracil

: 1-[(2S,3S,5S)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-3-phenylsulfanyl-tetrahydro-furan-2-yl]-1H-pyrimidine-2,4-dione

Guidance literature:: With tin(IV) chloride; Yield given. Multistep reaction. Yields of byproduct given; 1.) CH₂Cl₂, 0 deg C, 30 min, 2.) CH₂Cl₂, 0 deg C, 1 h;
DOI:10.3987/COM-93-6503