Technology Process of C23H25N5
There total 4 articles about C23H25N5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydroxylamine hydrochloride;
In
ethanol; water;
at 100 ℃;
for 24h;
DOI:10.1021/jm4000984
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C
1.2: 0.17 h / 0 °C
2.1: hydroxylamine hydrochloride / ethanol; water / 24 h / 100 °C
With
n-butyllithium; hydroxylamine hydrochloride;
In
tetrahydrofuran; ethanol; hexane; water;
DOI:10.1021/jm4000984
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 6 h / 80 °C
2.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C
2.2: 0.17 h / 0 °C
3.1: hydroxylamine hydrochloride / ethanol; water / 24 h / 100 °C
With
N-Bromosuccinimide; n-butyllithium; hydroxylamine hydrochloride; dibenzoyl peroxide;
In
tetrahydrofuran; tetrachloromethane; ethanol; hexane; water;
DOI:10.1021/jm4000984