tetra(o-tolyl)distibane

Base Information

Chemical Name:tetra(o-tolyl)distibane
CAS No.:189500-08-1
Molecular Formula:C₂₈H₂₈Sb₂
Molecular Weight:608.03
Hs Code.:

Synonyms:tetra(o-tolyl)distibane

Suppliers and Price of tetra(o-tolyl)distibane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of tetra(o-tolyl)distibane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tetra(o-tolyl)distibane

There total 2 articles about tetra(o-tolyl)distibane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.5%

: 23822-15-3
tri(o-tolyl)antimony

: 189500-08-1
tetra(o-tolyl)distibane

Guidance literature:: With Na; BrCH₂CH₂Br; In ammonia; NH3 (liquid); (Ar); o-Tol3Sb was added to soln. of Na in liq. NH3 at -70°C; mixt. was stirred for 1.5 h; BrCH2CH2Br was added dropwise through syringe;mixt. was stirred for 1 h; NH3 evapd.; washed (H2O); dried (vac.); crystd. (Et2O; -23°C); elem. anal.;
DOI:10.1016/S0022-328X(01)01466-8

Reference yield: 23.0%

: 166989-24-8
o-tolylbis(trimethylsilyl)antimony

: 189500-08-1
tetra(o-tolyl)distibane

: bis(di-o-tolylantimony)oxide

: (C₆H₄CH₃)2SbOSi(CH₃)3

: 165269-26-1
o-tolylantimony hexamer

: 23822-15-3
tri(o-tolyl)antimony

Guidance literature:: With O₂; In tetrahydrofuran; byproducts: ((CH3)3Si)2O; several days in air; other solvent: toluene, mesitylene, 1,4-dioxane andDMF; separation of crystals, washing (petroleum ether); elem. anal.;

Reference yield: 96.0%

: 189500-08-1
tetra(o-tolyl)distibane

: bis(di-o-tolylantimony)oxide

Guidance literature:: With air; In diethyl ether; (Ar); soln. of distibane in Et2O was exposed to air; solvent removed (vac.);
DOI:10.1016/S0022-328X(01)01466-8