5-acetamido-7,8,9-tri-O-acetyl-2,6-anhydro-4-(2-nitrobenzenesulfonamido)-3,4,5-trideoxy-D-glycero-D-galacto-non-2-enonic acid methyl ester

Base Information

Chemical Name:5-acetamido-7,8,9-tri-O-acetyl-2,6-anhydro-4-(2-nitrobenzenesulfonamido)-3,4,5-trideoxy-D-glycero-D-galacto-non-2-enonic acid methyl ester
CAS No.:1236306-91-4
Molecular Formula:C₂₄H₂₉N₃O₁₄S
Molecular Weight:615.572
Hs Code.:

Synonyms:5-acetamido-7,8,9-tri-O-acetyl-2,6-anhydro-4-(2-nitrobenzenesulfonamido)-3,4,5-trideoxy-D-glycero-D-galacto-non-2-enonic acid methyl ester

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Chemical Property of 5-acetamido-7,8,9-tri-O-acetyl-2,6-anhydro-4-(2-nitrobenzenesulfonamido)-3,4,5-trideoxy-D-glycero-D-galacto-non-2-enonic acid methyl ester

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Technology Process of 5-acetamido-7,8,9-tri-O-acetyl-2,6-anhydro-4-(2-nitrobenzenesulfonamido)-3,4,5-trideoxy-D-glycero-D-galacto-non-2-enonic acid methyl ester

There total 1 articles about 5-acetamido-7,8,9-tri-O-acetyl-2,6-anhydro-4-(2-nitrobenzenesulfonamido)-3,4,5-trideoxy-D-glycero-D-galacto-non-2-enonic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1694-92-4
2-Nitrobenzenesulfonyl chloride

: 139110-70-6
5-acetamido-7,8,9-tri-O-acetyl-2,6-anhydro-4-amino-3,4,5-trideoxy-D-glycero-D-galacto-non-2-enonic acid methyl ester

: 1236306-91-4
5-acetamido-7,8,9-tri-O-acetyl-2,6-anhydro-4-(2-nitrobenzenesulfonamido)-3,4,5-trideoxy-D-glycero-D-galacto-non-2-enonic acid methyl ester

Guidance literature:: In dichloromethane; at 20 ℃; for 6h; Inert atmosphere;
DOI:10.1016/j.bmc.2010.04.010

Reference yield:

: 58885-58-8
N-tert-butoxycarbonyl-3-aminopropanol

: 1236306-91-4
5-acetamido-7,8,9-tri-O-acetyl-2,6-anhydro-4-(2-nitrobenzenesulfonamido)-3,4,5-trideoxy-D-glycero-D-galacto-non-2-enonic acid methyl ester

: C₃₂H₄₄N₄O₁₆S

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 21h; Inert atmosphere;
DOI:10.1016/j.bmc.2010.04.010

Reference yield:

: 925-57-5
methyl 4-hydroxybutanoate

: 1236306-91-4
5-acetamido-7,8,9-tri-O-acetyl-2,6-anhydro-4-(2-nitrobenzenesulfonamido)-3,4,5-trideoxy-D-glycero-D-galacto-non-2-enonic acid methyl ester

: C₂₉H₃₇N₃O₁₆S

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 21h; Inert atmosphere;
DOI:10.1016/j.bmc.2010.04.010