8-chloro-1-(1-chloro-ethyl)-6-phenyl-4H-benzo[f][1,2,4]triazolo[4,3-a][1,4]diazepine

Base Information

Chemical Name:8-chloro-1-(1-chloro-ethyl)-6-phenyl-4H-benzo[f][1,2,4]triazolo[4,3-a][1,4]diazepine
CAS No.:39479-73-7
Molecular Formula:C₁₈H₁₄Cl₂N₄
Molecular Weight:357.242
Hs Code.:

8-chloro-1-(1-chloro-ethyl)-6-phenyl-4<i>H</i>-benzo[<i>f</i>][1,2,4]triazolo[4,3-<i>a</i>][1,4]diazepine

Synonyms:8-chloro-1-(1-chloro-ethyl)-6-phenyl-4H-benzo[f][1,2,4]triazolo[4,3-a][1,4]diazepine

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Chemical Property of 8-chloro-1-(1-chloro-ethyl)-6-phenyl-4H-benzo[f][1,2,4]triazolo[4,3-a][1,4]diazepine

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Technology Process of 8-chloro-1-(1-chloro-ethyl)-6-phenyl-4H-benzo[f][1,2,4]triazolo[4,3-a][1,4]diazepine

There total 3 articles about 8-chloro-1-(1-chloro-ethyl)-6-phenyl-4H-benzo[f][1,2,4]triazolo[4,3-a][1,4]diazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7623-09-8
2-chloropropionyl chloride

: 18091-89-9,112393-62-1
7-chloro-2-hydrazino-5-phenyl-3H-1,4-benzodiazepine

: 39479-73-7
8-chloro-1-(1-chloro-ethyl)-6-phenyl-4H-benzo[f][1,2,4]triazolo[4,3-a][1,4]diazepine

Guidance literature:: With sodium acetate; In acetic acid;

Reference yield:

: 2-Chloro-propionic acid N'-(7-chloro-5-phenyl-3H-benzo[e][1,4]diazepin-2-yl)-hydrazide

: 39479-73-7
8-chloro-1-(1-chloro-ethyl)-6-phenyl-4H-benzo[f][1,2,4]triazolo[4,3-a][1,4]diazepine

Guidance literature:: In acetic acid; for 0.333333h; Yield given; Heating;
DOI:10.1021/jm00178a009

Reference yield:

: 18091-89-9,112393-62-1
7-chloro-2-hydrazino-5-phenyl-3H-1,4-benzodiazepine

: 39479-73-7
8-chloro-1-(1-chloro-ethyl)-6-phenyl-4H-benzo[f][1,2,4]triazolo[4,3-a][1,4]diazepine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 1.58 h / 0 - 20 °C

2: acetic acid / 0.33 h / Heating

In tetrahydrofuran; acetic acid;
DOI:10.1021/jm00178a009