(S)-N-benzyloxycarbonyl-N-methyl-2-(4-hydroxybutanyl)-glycine benzyl ester

Base Information

Chemical Name:(S)-N-benzyloxycarbonyl-N-methyl-2-(4-hydroxybutanyl)-glycine benzyl ester
CAS No.:519156-54-8
Molecular Formula:C₂₂H₂₇NO₅
Molecular Weight:385.46
Hs Code.:

Synonyms:(S)-N-benzyloxycarbonyl-N-methyl-2-(4-hydroxybutanyl)-glycine benzyl ester

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Chemical Property of (S)-N-benzyloxycarbonyl-N-methyl-2-(4-hydroxybutanyl)-glycine benzyl ester

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Technology Process of (S)-N-benzyloxycarbonyl-N-methyl-2-(4-hydroxybutanyl)-glycine benzyl ester

There total 3 articles about (S)-N-benzyloxycarbonyl-N-methyl-2-(4-hydroxybutanyl)-glycine benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 100-39-0
benzyl bromide

: 519156-53-7
(S)-N-benzyloxycarbonyl-N-methyl-2-(4-hydroxybutanyl)-glycine

: 519156-54-8
(S)-N-benzyloxycarbonyl-N-methyl-2-(4-hydroxybutanyl)-glycine benzyl ester

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1021/jo026722l

Reference yield:

: 519156-49-1
(S)-4-(4-Acetoxy-butyl)-5-oxo-oxazolidine-3-carboxylic acid benzyl ester

: 519156-54-8
(S)-N-benzyloxycarbonyl-N-methyl-2-(4-hydroxybutanyl)-glycine benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / Et₃SiH; trifluoroacetic acid / CH₂Cl₂ / 48 h / 20 °C

2: 83 percent / aq. NaOH / 0 - 20 °C

3: 87 percent / K₂CO₃ / dimethylformamide / 20 °C

With triethylsilane; sodium hydroxide; potassium carbonate; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo026722l

Reference yield:

: 519156-52-6
(S)-N-benzyloxycarbonyl-N-methyl-2-(4-acetoxybutanyl)-glycine

: 519156-54-8
(S)-N-benzyloxycarbonyl-N-methyl-2-(4-hydroxybutanyl)-glycine benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / aq. NaOH / 0 - 20 °C

2: 87 percent / K₂CO₃ / dimethylformamide / 20 °C

With sodium hydroxide; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/jo026722l