(S)-2-benzyloxycarbonylamino-6-methanesulfonyloxy-hexanoic acid ethyl ester

Base Information

Chemical Name:(S)-2-benzyloxycarbonylamino-6-methanesulfonyloxy-hexanoic acid ethyl ester
CAS No.:921226-03-1
Molecular Formula:C₁₇H₂₅NO₇S
Molecular Weight:387.454
Hs Code.:

Synonyms:(S)-2-benzyloxycarbonylamino-6-methanesulfonyloxy-hexanoic acid ethyl ester

Suppliers and Price of (S)-2-benzyloxycarbonylamino-6-methanesulfonyloxy-hexanoic acid ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (S)-2-benzyloxycarbonylamino-6-methanesulfonyloxy-hexanoic acid ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (S)-2-benzyloxycarbonylamino-6-methanesulfonyloxy-hexanoic acid ethyl ester

There total 1 articles about (S)-2-benzyloxycarbonylamino-6-methanesulfonyloxy-hexanoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 124-63-0
methanesulfonyl chloride

: 475603-48-6
(S)-2-benzyloxycarbonylamino-6-hydroxyhexanoic acid ethyl ester

: 921226-03-1
(S)-2-benzyloxycarbonylamino-6-methanesulfonyloxy-hexanoic acid ethyl ester

Guidance literature:: With triethylamine; In dichloromethane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1039/c002796k

Reference yield:

: 921226-03-1
(S)-2-benzyloxycarbonylamino-6-methanesulfonyloxy-hexanoic acid ethyl ester

: 90877-70-6,4977-62-2
ethyl 2-acetamido-2-cyanoacetate

: 921226-08-6
diethyl 2-acetamido-7-(benzyloxycarbonylamino)-2-cyanooctanedioate

Guidance literature:: ethyl 2-acetamido-2-cyanoacetate; With sodium ethanolate; In ethanol; at 60 ℃; for 0.5h;

(S)-2-benzyloxycarbonylamino-6-methanesulfonyloxy-hexanoic acid ethyl ester; In ethanol; Heating;
DOI:10.1021/ja066002m

Reference yield:

: 921226-03-1
(S)-2-benzyloxycarbonylamino-6-methanesulfonyloxy-hexanoic acid ethyl ester

: diethyl 10-acetamido-15,15-dimethyl-3,13-dioxo-1-phenyl-2,14-dioxa-4,12-diazahexadecane-5,10-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaOEt / ethanol / 0.5 h / 60 °C

1.2: ethanol / Heating

2.1: NiCl₂*6H₂O; NaBH₄ / methanol / 0 - 20 °C

With sodium tetrahydroborate; sodium ethanolate; nickel dichloride; In methanol; ethanol;
DOI:10.1021/ja066002m