(4S)-1-(2-bromo-2,2-difluoroethyl)-4-(2-bromoisopropyl)-cyclohexene

Base Information

Chemical Name:(4S)-1-(2-bromo-2,2-difluoroethyl)-4-(2-bromoisopropyl)-cyclohexene
CAS No.:1070912-72-9
Molecular Formula:C₁₁H₁₆Br₂F₂
Molecular Weight:346.053
Hs Code.:

Synonyms:(4S)-1-(2-bromo-2,2-difluoroethyl)-4-(2-bromoisopropyl)-cyclohexene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4S)-1-(2-bromo-2,2-difluoroethyl)-4-(2-bromoisopropyl)-cyclohexene

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Technology Process of (4S)-1-(2-bromo-2,2-difluoroethyl)-4-(2-bromoisopropyl)-cyclohexene

There total 2 articles about (4S)-1-(2-bromo-2,2-difluoroethyl)-4-(2-bromoisopropyl)-cyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 56-23-5
tetrachloromethane

: 18172-67-3,19902-08-0,25719-60-2
beta-pinene

: 1070912-72-9
(4S)-1-(2-bromo-2,2-difluoroethyl)-4-(2-bromoisopropyl)-cyclohexene

Guidance literature:: With C₃₀H₂₆N₆Ru⁽²⁺⁾*2Cl^(1-); In dimethyl sulfoxide; Inert atmosphere; Irradiation;
DOI:10.1021/ja300798k

Reference yield: 90.0%

: 75-61-6
dibromodifluoromethane

: 18172-67-3,19902-08-0,25719-60-2
beta-pinene

: 1070912-72-9
(4S)-1-(2-bromo-2,2-difluoroethyl)-4-(2-bromoisopropyl)-cyclohexene

Guidance literature:: With sodium dithionite; sodium hydrogencarbonate; In water; acetonitrile; at 18 - 20 ℃; for 0.5h;
DOI:10.1016/j.jfluchem.2007.07.004

Reference yield:

: 1070912-72-9
(4S)-1-(2-bromo-2,2-difluoroethyl)-4-(2-bromoisopropyl)-cyclohexene

: 1070912-81-0
1-(2,2-difluorovinyl)-4-isopropylcyclohexene

: 1070912-79-6
4-(2-bromo-2,2-difluoroethyl)-1-isopropylcyclohexene

: 1070912-80-9
4-(2-bromo-2,2-difluoroethyl)-1-isopropylcyclohexane

Guidance literature:: (4S)-1-(2-bromo-2,2-difluoroethyl)-4-(2-bromoisopropyl)-cyclohexene; With 2,2,6,6-tetramethyl-piperidine; In toluene; for 48h; Heating;

With hydrogen; palladium on activated charcoal; In ethyl acetate; at 20 ℃; for 4h; under 1275.13 Torr;

In tetrahydrofuran; at 20 ℃; for 2h; Further stages. Title compound not separated from byproducts.;
DOI:10.1016/j.jfluchem.2007.07.004