C₂₂H₃₈IN₃

Base Information

Chemical Name:C₂₂H₃₈IN₃
CAS No.:949079-72-5
Molecular Formula:C₂₂H₃₈IN₃
Molecular Weight:471.468
Hs Code.:

C<sub>22</sub>H<sub>38</sub>IN<sub>3</sub>

Synonyms:C₂₂H₃₈IN₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₃₈IN₃

Chemical Property:

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Technology Process of C₂₂H₃₈IN₃

There total 3 articles about C₂₂H₃₈IN₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 314732-79-1
1-amino-2,5-di-n-hexyl-4-iodobenzene

: 109-89-7
diethylamine

: 949079-72-5
C₂₂H₃₈IN₃

Guidance literature:: With t-butylnitrite; boron trifluoride diethyl etherate; potassium carbonate; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1016/j.tet.2007.05.116

Reference yield:

: 949079-71-4
C₂₀H₃₂ION

: 949079-72-5
C₂₂H₃₈IN₃

Guidance literature:: Multi-step reaction with 2 steps

1: aq. HCl / ethanol / 5 h / 85 °C

2: 92 percent / BF₃*Et₂O; t-BuNO; K₂CO₃ / CH₂Cl₂ / 1 h / 20 °C

With hydrogenchloride; t-butylnitrite; boron trifluoride diethyl etherate; potassium carbonate; In ethanol; dichloromethane;
DOI:10.1016/j.tet.2007.05.116

Reference yield:

: 162715-91-5
1,4-dihexyl-2,5-diiodobenzene

: 949079-72-5
C₂₂H₃₈IN₃

Guidance literature:: Multi-step reaction with 3 steps

1: 59 percent / K₃PO₄; N,N'-dimethylethylenediamine; CuI / dimethylformamide / 24 h / 80 °C

2: aq. HCl / ethanol / 5 h / 85 °C

3: 92 percent / BF₃*Et₂O; t-BuNO; K₂CO₃ / CH₂Cl₂ / 1 h / 20 °C

With hydrogenchloride; potassium phosphate; copper(l) iodide; t-butylnitrite; boron trifluoride diethyl etherate; potassium carbonate; N,N`-dimethylethylenediamine; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2007.05.116