(+)-(1S)-2-(3,5-dimethoxy-4-(8-methoxy-1-methoxymethoxy-3-methylnaphthalen-2-yl)-phenyl)-1-methylethylamine

Base Information

Chemical Name:(+)-(1S)-2-(3,5-dimethoxy-4-(8-methoxy-1-methoxymethoxy-3-methylnaphthalen-2-yl)-phenyl)-1-methylethylamine
CAS No.:403706-09-2
Molecular Formula:C₂₅H₃₁NO₅
Molecular Weight:425.525
Hs Code.:

Synonyms:(+)-(1S)-2-(3,5-dimethoxy-4-(8-methoxy-1-methoxymethoxy-3-methylnaphthalen-2-yl)-phenyl)-1-methylethylamine

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Chemical Property of (+)-(1S)-2-(3,5-dimethoxy-4-(8-methoxy-1-methoxymethoxy-3-methylnaphthalen-2-yl)-phenyl)-1-methylethylamine

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Technology Process of (+)-(1S)-2-(3,5-dimethoxy-4-(8-methoxy-1-methoxymethoxy-3-methylnaphthalen-2-yl)-phenyl)-1-methylethylamine

There total 10 articles about (+)-(1S)-2-(3,5-dimethoxy-4-(8-methoxy-1-methoxymethoxy-3-methylnaphthalen-2-yl)-phenyl)-1-methylethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 403706-19-4
(1S)-2-{2-(3,5-dimethoxy-4-(8-methoxy-1-methoxymethoxy-3-methylnaphthalen-2-yl)-phenyl)-1-methylethyl}isoindole-1,3-dione

: 403706-09-2
(+)-(1S)-2-(3,5-dimethoxy-4-(8-methoxy-1-methoxymethoxy-3-methylnaphthalen-2-yl)-phenyl)-1-methylethylamine

Guidance literature:: With methylamine; In ethanol; for 1h; Heating;
DOI:10.1021/jo0611364

Reference yield:

: 403706-13-8
(+)-(2R,3R)-{3-(3,5-dimethoxy-4-(8-methoxy-1-methoxymethoxy-3-methylnaphthalen-2-yl)-phenyl)-2,3-oxiranyl}methanol

: 403706-09-2
(+)-(1S)-2-(3,5-dimethoxy-4-(8-methoxy-1-methoxymethoxy-3-methylnaphthalen-2-yl)-phenyl)-1-methylethylamine

Guidance literature:: Multi-step reaction with 4 steps

1: 83 percent / Et₃N; DMAP / CH₂Cl₂ / 1 h / 0 °C

2: 94 percent / LiAlH₄ / tetrahydrofuran / 2.5 h / 0 - 20 °C

3: 82 percent / PPh₃; DEAD / tetrahydrofuran / 0 - 20 °C

4: 100 percent / aq. MeNH₂ / ethanol / 1 h / Heating

With dmap; lithium aluminium tetrahydride; triethylamine; triphenylphosphine; methylamine; diethylazodicarboxylate; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/jo0611364

Reference yield:

: 403706-14-9
(+)-(2R,3R)-toluene-4-sulfonic acid 3-(3,5-dimethoxy-4-(8-methoxy-1-methoxymethoxy-3-methylnaphthalen-2-yl)-phenyl)-2,3-oxiranylmethyl ester

: 403706-09-2
(+)-(1S)-2-(3,5-dimethoxy-4-(8-methoxy-1-methoxymethoxy-3-methylnaphthalen-2-yl)-phenyl)-1-methylethylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / LiAlH₄ / tetrahydrofuran / 2.5 h / 0 - 20 °C

2: 82 percent / PPh₃; DEAD / tetrahydrofuran / 0 - 20 °C

3: 100 percent / aq. MeNH₂ / ethanol / 1 h / Heating

With lithium aluminium tetrahydride; triphenylphosphine; methylamine; diethylazodicarboxylate; In tetrahydrofuran; ethanol;
DOI:10.1021/jo0611364