O-(L-N-(benzyloxycarbonyl)-N,O-dimethyltyrosyl)-N-(tert-butoxycarbonyl)-L-serine

Base Information

Chemical Name:O-(L-N-(benzyloxycarbonyl)-N,O-dimethyltyrosyl)-N-(tert-butoxycarbonyl)-L-serine
CAS No.:945473-49-4
Molecular Formula:C₂₇H₃₄N₂O₉
Molecular Weight:530.575
Hs Code.:

Synonyms:O-(L-N-(benzyloxycarbonyl)-N,O-dimethyltyrosyl)-N-(tert-butoxycarbonyl)-L-serine

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Chemical Property of O-(L-N-(benzyloxycarbonyl)-N,O-dimethyltyrosyl)-N-(tert-butoxycarbonyl)-L-serine

Chemical Property:

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Technology Process of O-(L-N-(benzyloxycarbonyl)-N,O-dimethyltyrosyl)-N-(tert-butoxycarbonyl)-L-serine

There total 3 articles about O-(L-N-(benzyloxycarbonyl)-N,O-dimethyltyrosyl)-N-(tert-butoxycarbonyl)-L-serine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 945473-75-6
O-(L-N-(benzyloxycarbonyl)-N,O-dimethyltyrosyl)-N-(tert-butoxycarbonyl)-L-serine phenacyl ester

: 945473-49-4
O-(L-N-(benzyloxycarbonyl)-N,O-dimethyltyrosyl)-N-(tert-butoxycarbonyl)-L-serine

Guidance literature:: With acetic acid; zinc; In water; at 0 ℃; for 3h;
DOI:10.1021/jo070412r

Reference yield:

: 3262-72-4
(S)-N-(tert-butoxycarbonyl)serine

: 945473-49-4
O-(L-N-(benzyloxycarbonyl)-N,O-dimethyltyrosyl)-N-(tert-butoxycarbonyl)-L-serine

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / triethylamine / ethyl acetate / 48 h / 20 °C

2: 63 percent / 4-(dimethylamino)pyridine; N,N'-dicyclohexylcarbodiimide / CH₂Cl₂ / 20 °C

3: 75 percent / Zn; acetic acid / H₂O / 3 h / 0 °C

With dmap; acetic acid; triethylamine; dicyclohexyl-carbodiimide; zinc; In dichloromethane; water; ethyl acetate;
DOI:10.1021/jo070412r

Reference yield:

: 120219-31-0
L-N-(tert-butoxycarbonyl)serine phenacyl ester

: 945473-49-4
O-(L-N-(benzyloxycarbonyl)-N,O-dimethyltyrosyl)-N-(tert-butoxycarbonyl)-L-serine

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / 4-(dimethylamino)pyridine; N,N'-dicyclohexylcarbodiimide / CH₂Cl₂ / 20 °C

2: 75 percent / Zn; acetic acid / H₂O / 3 h / 0 °C

With dmap; acetic acid; dicyclohexyl-carbodiimide; zinc; In dichloromethane; water;
DOI:10.1021/jo070412r