Technology Process of 4-p-tolyl-7-[4-(4-vinylbenzyloxy)phenyl]-2,1,3-benzothiadiazole
There total 5 articles about 4-p-tolyl-7-[4-(4-vinylbenzyloxy)phenyl]-2,1,3-benzothiadiazole which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
N,N-dimethyl-formamide; acetonitrile;
at 65 ℃;
for 4h;
DOI:10.1021/ma1008572
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hexadecyldibutylphosphonium bromide; hydrogen bromide / 20 h / 130 °C
2: potassium carbonate / N,N-dimethyl-formamide; acetonitrile / 4 h / 65 °C
With
hexadecyldibutylphosphonium bromide; hydrogen bromide; potassium carbonate;
In
N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ma1008572
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / tetrahydrofuran; water; toluene / 20 h / 85 °C
2: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / tetrahydrofuran; water; toluene / 24 h / 85 °C
3: hexadecyldibutylphosphonium bromide; hydrogen bromide / 20 h / 130 °C
4: potassium carbonate / N,N-dimethyl-formamide; acetonitrile / 4 h / 65 °C
With
tetrakis(triphenylphosphine) palladium(0); hexadecyldibutylphosphonium bromide; hydrogen bromide; sodium carbonate; potassium carbonate;
In
tetrahydrofuran; water; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1021/ma1008572
