benzoxazol-2-yl 2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:benzoxazol-2-yl 2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-1-thio-β-D-glucopyranoside
CAS No.:1117896-25-9
Molecular Formula:C₆₈H₅₃NO₁₈S
Molecular Weight:1204.23
Hs Code.:

Synonyms:benzoxazol-2-yl 2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-1-thio-β-D-glucopyranoside

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Chemical Property of benzoxazol-2-yl 2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-1-thio-β-D-glucopyranoside

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Technology Process of benzoxazol-2-yl 2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-1-thio-β-D-glucopyranoside

There total 3 articles about benzoxazol-2-yl 2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 862537-77-7
benzoxazol-2-yl 2,3,4-tri-O-benzoyl-1-thio-β-D-glucopyranoside

: 744245-92-9
2-thiazolinyl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside

: 1117896-25-9
benzoxazol-2-yl 2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-1-thio-β-D-glucopyranoside

Guidance literature:: With benzyl bromide; In 1,2-dichloro-ethane; at 55 ℃; for 24h; Inert atmosphere; Molecular sieve;
DOI:10.1021/ol802740b

Reference yield: 69.0%

: 635727-37-6
2-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosylmercapto)-1,3-benzoxazole

: 810670-84-9
4,5-dihydrothiazol-2-yl 2,3,4-tri-O-benzoyl-1-thio-β-D-glucopyranoside

: 1117896-25-9
benzoxazol-2-yl 2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-1-thio-β-D-glucopyranoside

Guidance literature:: With bismuth(lll) trifluoromethanesulfonate; In 1,2-dichloro-ethane; at 0 - 20 ℃; for 24h; Inert atmosphere; Molecular sieve;
DOI:10.1021/ol802740b

Reference yield: 54.0%

: 862537-77-7
benzoxazol-2-yl 2,3,4-tri-O-benzoyl-1-thio-β-D-glucopyranoside

: 105376-04-3,138661-53-7,113214-71-4
ethyl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside

: 1117896-25-9
benzoxazol-2-yl 2,3,4-tri-O-benzoyl-6-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-1-thio-β-D-glucopyranoside

Guidance literature:: benzoxazol-2-yl 2,3,4-tri-O-benzoyl-1-thio-β-D-glucopyranoside; ethyl 2,3,4,6-tetra-O-benzoyl-1-thio-β-D-glucopyranoside; In 1,2-dichloro-ethane; at 20 ℃; for 1h; Molecular sieve; Inert atmosphere;

With dimethyl-(methylthio)-sulphonium trifluoromethanesulphonate; In 1,2-dichloro-ethane; at 0 - 20 ℃; Inert atmosphere; Molecular sieve;
DOI:10.1021/jo201117s