2-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosylmercapto)-1,3-benzoxazole

Base Information

Chemical Name:2-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosylmercapto)-1,3-benzoxazole
CAS No.:635727-37-6
Molecular Formula:C₄₁H₃₁NO₁₀S
Molecular Weight:729.764
Hs Code.:

Synonyms:2-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosylmercapto)-1,3-benzoxazole

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Chemical Property of 2-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosylmercapto)-1,3-benzoxazole

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Technology Process of 2-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosylmercapto)-1,3-benzoxazole

There total 3 articles about 2-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosylmercapto)-1,3-benzoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 98-88-4
benzoyl chloride

: 91958-78-0
2-(β-D-glucopyranosylmercapto)-1,3-benzoxazole

: 635727-37-6
2-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosylmercapto)-1,3-benzoxazole

Guidance literature:: With pyridine;
DOI:10.1021/jo071191s

Reference yield: 35.0%

: 627466-64-2
2,3,4,6-tetra-O-benzoyl-D-glucopyranose

: 2382-96-9,118090-08-7
2-sulfanyl-1,3-benzoxazole

: 2-(2',3',4',6'-tetra-O-benzoyl-1-thio-α-D-glucopyranosyl)benzoxazole

: 2-thioxo-3-(2',3',4',6'-tetra-O-benzoyl-α-D-glucopyranosyl)benzoxazole

: 635727-37-6
2-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosylmercapto)-1,3-benzoxazole

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at -50 - -10 ℃; for 14h;
DOI:10.1021/ol701466u

Reference yield:

: 6044-27-5
benzoxazol-2-yl 2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranoside

: 635727-37-6
2-(2',3',4',6'-tetra-O-benzoyl-β-D-glucopyranosylmercapto)-1,3-benzoxazole

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / NH₃; MeOH / 16 h / 20 °C

2: 88 percent / pyridine

With pyridine; methanol; ammonia;
DOI:10.1021/jo071191s