4-(3,4-methylenedioxyphenyl)-4-oxo-2-(3,4,5-trimethoxyphenyl)butyric acid

Base Information

• Chemical Name: 4-(3,4-methylenedioxyphenyl)-4-oxo-2-(3,4,5-trimethoxyphenyl)butyric acid
• CAS No.: 88775-29-5
• Molecular Formula: C₂₀H₂₀O₈
• Molecular Weight: 388.374

Synonyms:4-(3,4-methylenedioxyphenyl)-4-oxo-2-(3,4,5-trimethoxyphenyl)butyric acid

Chemical Property of 4-(3,4-methylenedioxyphenyl)-4-oxo-2-(3,4,5-trimethoxyphenyl)butyric acid

Chemical Property:

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Technology Process of 4-(3,4-methylenedioxyphenyl)-4-oxo-2-(3,4,5-trimethoxyphenyl)butyric acid

There total 2 articles about 4-(3,4-methylenedioxyphenyl)-4-oxo-2-(3,4,5-trimethoxyphenyl)butyric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

4-(3,4-methylenedioxyphenyl)-4-oxo-2-(3,4,5-trimethoxyphenyl)butyramide (88775-41-1) → 1-(benzo[d][1,3]dioxol-6-yl)ethanone (3162-29-6) + (Z)-2-(3,4,5-trimethoxyphenyl)-4-(3,4-methylenedioxyphenyl)-4-oxo-2-butenoic acid (88775-49-9) + 4-(3,4-methylenedioxyphenyl)-4-oxo-2-(3,4,5-trimethoxyphenyl)butyric acid (88775-29-5) + Eudesmic acid (118-41-2)

Guidance literature:

With sodium hydroxide; In ethanol; for 10h; Product distribution; Heating; var. condition;

DOI:10.1248/cpb.31.3039

Reference yield:

4-(3,4-methylenedioxyphenyl)-4-oxo-2-(3,4,5-trimethoxyphenyl)butyronitrile (88775-24-0) → 4-(3,4-methylenedioxyphenyl)-4-oxo-2-(3,4,5-trimethoxyphenyl)butyric acid (88775-29-5)

Guidance literature:

With sodium hydroxide; In ethanol; for 11h; Heating;

DOI:10.1248/cpb.31.3039

Reference yield:

4-(3,4-methylenedioxyphenyl)-4-oxo-2-(3,4,5-trimethoxyphenyl)butyric acid (88775-29-5) → 4-(3,4-methylenedioxyphenyl)-2-(3,4,5-trimethoxyphenyl)butyric acid (88775-32-0)

Guidance literature:

With hydrogen; pyrographite; palladium dichloride; In acetic acid; Ambient temperature;

DOI:10.1248/cpb.31.3039

upstream raw materials:

4-(3,4-methylenedioxyphenyl)-4-oxo-2-(3,4,5-trimethoxyphenyl)butyronitrile

4-(3,4-methylenedioxyphenyl)-4-oxo-2-(3,4,5-trimethoxyphenyl)butyramide

Downstream raw materials:

4-(3,4-methylenedioxyphenyl)-2-(3,4,5-trimethoxyphenyl)butyric acid

6,7-methylenedioxy-2-(3,4,5-trimethoxyphenyl)-3,4-dihydronaphthalen-1(2H)-one

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