(acac)2Ru(II)(μ-3,6-bis(3,5-dimethylpyrazolyl)-1,2,4,5-tetrazine)Ru(II)(acac)2

Base Information

Chemical Name:(acac)2Ru(II)(μ-3,6-bis(3,5-dimethylpyrazolyl)-1,2,4,5-tetrazine)Ru(II)(acac)2
CAS No.:774198-39-9
Molecular Formula:C₃₂H₄₂N₈O₈Ru₂
Molecular Weight:868.874
Hs Code.:

Synonyms:(acac)2Ru(II)(μ-3,6-bis(3,5-dimethylpyrazolyl)-1,2,4,5-tetrazine)Ru(II)(acac)2

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Chemical Property of (acac)2Ru(II)(μ-3,6-bis(3,5-dimethylpyrazolyl)-1,2,4,5-tetrazine)Ru(II)(acac)2

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Technology Process of (acac)2Ru(II)(μ-3,6-bis(3,5-dimethylpyrazolyl)-1,2,4,5-tetrazine)Ru(II)(acac)2

There total 1 articles about (acac)2Ru(II)(μ-3,6-bis(3,5-dimethylpyrazolyl)-1,2,4,5-tetrazine)Ru(II)(acac)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 30169-25-6
3,6-bis-(3,5-dimethyl-pyrazol-1-yl)-1,2,4,5-tetrazine

: bis(acetonitrile)bis(2,4-pentanedionato)ruthenium(II)

: 31378-26-4,31378-27-5,14284-93-6
tris(2,4-pentanedionato)ruthenium(III)

: 774198-39-9
(acac)2Ru(II)(μ-3,6-bis(3,5-dimethylpyrazolyl)-1,2,4,5-tetrazine)Ru(II)(acac)2

: [(acac)2Ru(II)(μ-3,6-bis(3,5-dimethylpyrazolyl)-1,2,4,5-tetrazine)Ru(II)(acac)2](ClO4)

Guidance literature:: In ethanol; under N2; Ru complex and ligand (molar ratio 2:1) in EtOH heated to reflux for 12 h; solvent reduced; kept in deep freezer overnight; filtered; ppt. washed (cold EtOH), dissolved in MeCN, aq. NaClO4 (excess) added, kept in deep freezer overnight; filtered, ppt. washed (cold H2O, cold EtOH), dried under vac. (Ru(II)Ru(III) complex); filtrate (1st filtration) evapd. to dryness; dissolved inCH2Cl2 (Ru(II)Ru(II) complex); both compds. sepd. by column chromy.; ev apd.; elem. anal.;
DOI:10.1021/ic049346r