undec-10-enoic acid 4-(6-tert-butoxycarbonylamino-hexylcarbamoyl)-2-nitro-benzyl ester

Base Information

• Chemical Name: undec-10-enoic acid 4-(6-tert-butoxycarbonylamino-hexylcarbamoyl)-2-nitro-benzyl ester
• CAS No.: 870074-59-2
• Molecular Formula: C₃₀H₄₇N₃O₇
• Molecular Weight: 561.719

Synonyms:undec-10-enoic acid 4-(6-tert-butoxycarbonylamino-hexylcarbamoyl)-2-nitro-benzyl ester

Chemical Property of undec-10-enoic acid 4-(6-tert-butoxycarbonylamino-hexylcarbamoyl)-2-nitro-benzyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of undec-10-enoic acid 4-(6-tert-butoxycarbonylamino-hexylcarbamoyl)-2-nitro-benzyl ester

There total 3 articles about undec-10-enoic acid 4-(6-tert-butoxycarbonylamino-hexylcarbamoyl)-2-nitro-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.9%

[6-(4-(hydroxymethyl)-3-nitrobenzoylamino)hexyl]carbamic acid tert-butyl ester (870074-58-1) + 10-undecenoic acid (112-38-9) → undec-10-enoic acid 4-(6-tert-butoxycarbonylamino-hexylcarbamoyl)-2-nitro-benzyl ester (870074-59-2)

Guidance literature:

10-undecenoic acid; With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; In dichloromethane; at 20 ℃; for 0.5h;

[6-(4-(hydroxymethyl)-3-nitrobenzoylamino)hexyl]carbamic acid tert-butyl ester; With triethylamine; In dichloromethane;

DOI:10.1021/ja054666a

Reference yield:

tert-butyl N-(6-aminohexyl)carbamate (51857-17-1) → undec-10-enoic acid 4-(6-tert-butoxycarbonylamino-hexylcarbamoyl)-2-nitro-benzyl ester (870074-59-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 55.9 percent / N-(3-dimethylaminopropyl)-N'-ethylcarbodiimide*HCl / ethanol / 0 - 20 °C

2.1: (benzotriazol-1-yloxy)tris(dimethylamino)phosphonium*PF₆ / CH₂Cl₂ / 0.5 h / 20 °C

2.2: 67.9 percent / triethylamine / CH₂Cl₂

With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In ethanol; dichloromethane;

DOI:10.1021/ja054666a

Reference yield:

4-(hydroxymethyl)-3-nitrobenzoic acid (82379-38-2) → undec-10-enoic acid 4-(6-tert-butoxycarbonylamino-hexylcarbamoyl)-2-nitro-benzyl ester (870074-59-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 55.9 percent / N-(3-dimethylaminopropyl)-N'-ethylcarbodiimide*HCl / ethanol / 0 - 20 °C

2.1: (benzotriazol-1-yloxy)tris(dimethylamino)phosphonium*PF₆ / CH₂Cl₂ / 0.5 h / 20 °C

2.2: 67.9 percent / triethylamine / CH₂Cl₂

With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In ethanol; dichloromethane;

DOI:10.1021/ja054666a

upstream raw materials:

[6-(4-(hydroxymethyl)-3-nitrobenzoylamino)hexyl]carbamic acid tert-butyl ester

10-undecenoic acid

tert-butyl N-(6-aminohexyl)carbamate

4-(hydroxymethyl)-3-nitrobenzoic acid

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 870074-59-2 undec-10-enoic acid 4-(6-tert-butoxycarbonylamino-hexylcarbamoyl)-2-nitro-benzyl ester

Send

Send

Metric Ton KG G Pound L ML

Send

Send