1,1-dimethylethyl methyl{(1S)-2-({[(phenylmethyl)oxy]carbonyl}amino)-1-[(3R)-tetrahydro-2H-pyran-3-ylmethyl]ethyl}carbamate

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Chemical Name:1,1-dimethylethyl methyl{(1S)-2-({[(phenylmethyl)oxy]carbonyl}amino)-1-[(3R)-tetrahydro-2H-pyran-3-ylmethyl]ethyl}carbamate
CAS No.:1093865-03-2
Molecular Formula:C₂₂H₃₄N₂O₅
Molecular Weight:406.522
Hs Code.:

Synonyms:1,1-dimethylethyl methyl{(1S)-2-({[(phenylmethyl)oxy]carbonyl}amino)-1-[(3R)-tetrahydro-2H-pyran-3-ylmethyl]ethyl}carbamate

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Chemical Property of 1,1-dimethylethyl methyl{(1S)-2-({[(phenylmethyl)oxy]carbonyl}amino)-1-[(3R)-tetrahydro-2H-pyran-3-ylmethyl]ethyl}carbamate

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Technology Process of 1,1-dimethylethyl methyl{(1S)-2-({[(phenylmethyl)oxy]carbonyl}amino)-1-[(3R)-tetrahydro-2H-pyran-3-ylmethyl]ethyl}carbamate

There total 3 articles about 1,1-dimethylethyl methyl{(1S)-2-({[(phenylmethyl)oxy]carbonyl}amino)-1-[(3R)-tetrahydro-2H-pyran-3-ylmethyl]ethyl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1093865-02-1
1,1-dimethylethyl methyl{2-({[(phenylmethyl)oxy]carbonyl}amino)-1-[(3R)-tetrahydro-2H-pyran-3-ylmethyl]ethyl}carbamate

: 1093865-03-2
1,1-dimethylethyl methyl{(1S)-2-({[(phenylmethyl)oxy]carbonyl}amino)-1-[(3R)-tetrahydro-2H-pyran-3-ylmethyl]ethyl}carbamate

: 1093865-04-3
1,1-dimethylethyl methyl{(1R)-2-({[(phenylmethyl)oxy]carbonyl}amino)-1-[(3R)-tetrahydro-2H-pyran-3-ylmethyl]ethyl}carbamate

Guidance literature:: In hexane; diethylamine; isopropyl alcohol; Purification / work up; Resolution of racemate;

Reference yield:

: 1093865-64-5
1,1-dimethylethyl {2-amino-1-[(3R)-tetrahydro-2H-pyran-3-ylmethyl]ethyl}methylcarbamate

: 501-53-1,94274-21-2
benzyl chloroformate

: 1093865-03-2
1,1-dimethylethyl methyl{(1S)-2-({[(phenylmethyl)oxy]carbonyl}amino)-1-[(3R)-tetrahydro-2H-pyran-3-ylmethyl]ethyl}carbamate

: 1093865-04-3
1,1-dimethylethyl methyl{(1R)-2-({[(phenylmethyl)oxy]carbonyl}amino)-1-[(3R)-tetrahydro-2H-pyran-3-ylmethyl]ethyl}carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 0 °C

2: hexane; diethylamine; isopropyl alcohol / Resolution of racemate

With N-ethyl-N,N-diisopropylamine; In hexane; dichloromethane; diethylamine; isopropyl alcohol;

Reference yield:

: 1093865-64-5
1,1-dimethylethyl {2-amino-1-[(3R)-tetrahydro-2H-pyran-3-ylmethyl]ethyl}methylcarbamate

: 1093865-03-2
1,1-dimethylethyl methyl{(1S)-2-({[(phenylmethyl)oxy]carbonyl}amino)-1-[(3R)-tetrahydro-2H-pyran-3-ylmethyl]ethyl}carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 0 °C

2: hexane; diethylamine; isopropyl alcohol / Resolution of racemate

With N-ethyl-N,N-diisopropylamine; In hexane; dichloromethane; diethylamine; isopropyl alcohol;