3-(2-fluorophenyl)-6,7-dimethoxy-1-(4-methoxyphenyl)-1H-benzo[g]indazole

Base Information

Chemical Name:3-(2-fluorophenyl)-6,7-dimethoxy-1-(4-methoxyphenyl)-1H-benzo[g]indazole
CAS No.:1394914-03-4
Molecular Formula:C₂₆H₂₁FN₂O₃
Molecular Weight:428.463
Hs Code.:

Synonyms:3-(2-fluorophenyl)-6,7-dimethoxy-1-(4-methoxyphenyl)-1H-benzo[g]indazole

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Chemical Property of 3-(2-fluorophenyl)-6,7-dimethoxy-1-(4-methoxyphenyl)-1H-benzo[g]indazole

Chemical Property:

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Technology Process of 3-(2-fluorophenyl)-6,7-dimethoxy-1-(4-methoxyphenyl)-1H-benzo[g]indazole

There total 6 articles about 3-(2-fluorophenyl)-6,7-dimethoxy-1-(4-methoxyphenyl)-1H-benzo[g]indazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₆H₂₃FN₂O₄

: 1394914-03-4
3-(2-fluorophenyl)-6,7-dimethoxy-1-(4-methoxyphenyl)-1H-benzo[g]indazole

Guidance literature:: With acetic acid; In tetrahydrofuran; water; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.tet.2012.07.011

Reference yield:

: 1394913-90-6
5-(2-allyl-3,4-dimethoxyphenyl)-3-(2-fluorophenyl)-1-(4-methoxyphenyl)-1H-pyrazole

: 1394914-03-4
3-(2-fluorophenyl)-6,7-dimethoxy-1-(4-methoxyphenyl)-1H-benzo[g]indazole

Guidance literature:: Multi-step reaction with 3 steps

1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

2: sodium periodate / tetrahydrofuran; water / 1 h / 20 °C / Inert atmosphere

3: acetic acid / tetrahydrofuran; water / 1 h / 20 °C / Inert atmosphere

With sodium periodate; osmium(VIII) oxide; water; acetic acid; 4-methylmorpholine N-oxide; In tetrahydrofuran; water;
DOI:10.1016/j.tet.2012.07.011

Reference yield:

: C₂₇H₂₇FN₂O₃

: 1394914-03-4
3-(2-fluorophenyl)-6,7-dimethoxy-1-(4-methoxyphenyl)-1H-benzo[g]indazole

Guidance literature:: Multi-step reaction with 4 steps

1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 3 h / Inert atmosphere; Reflux

2: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

3: sodium periodate / tetrahydrofuran; water / 1 h / 20 °C / Inert atmosphere

4: acetic acid / tetrahydrofuran; water / 1 h / 20 °C / Inert atmosphere

With sodium periodate; osmium(VIII) oxide; water; acetic acid; 4-methylmorpholine N-oxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; water; toluene;
DOI:10.1016/j.tet.2012.07.011