isopropyl (S)-2-tert-butoxycarbonylamino-3-phenylpropanoate

Base Information

Chemical Name:isopropyl (S)-2-tert-butoxycarbonylamino-3-phenylpropanoate
CAS No.:247178-99-0
Molecular Formula:C₁₇H₂₅NO₄
Molecular Weight:307.39
Hs Code.:

Synonyms:isopropyl (S)-2-tert-butoxycarbonylamino-3-phenylpropanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of isopropyl (S)-2-tert-butoxycarbonylamino-3-phenylpropanoate

Chemical Property:

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Technology Process of isopropyl (S)-2-tert-butoxycarbonylamino-3-phenylpropanoate

There total 3 articles about isopropyl (S)-2-tert-butoxycarbonylamino-3-phenylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 955379-49-4
isopropyl 2-((tert-butoxycarbonyl)amino)acrylate

: 960-16-7
tributylphenylstannane

: 1026133-82-3
isopropyl (R)-2-tert-butoxycarbonylamino-3-phenylpropanoate

: 247178-99-0
isopropyl (S)-2-tert-butoxycarbonylamino-3-phenylpropanoate

Guidance literature:: With 2-methoxy-phenol; bis(1,5-cyclooctadiene)rhodium(I) hexafluorophosphate; (S)-(1,1'-binaphthalene)-2,2'-diylbis(diphenylphosphine); In toluene; at 110 - 115 ℃; for 20h; Title compound not separated from byproducts.;
DOI:10.1021/ja710691p

Reference yield:

: 955379-49-4
isopropyl 2-((tert-butoxycarbonyl)amino)acrylate

: potassium phenyltrifluoborate

: 1026133-82-3
isopropyl (R)-2-tert-butoxycarbonylamino-3-phenylpropanoate

: 247178-99-0
isopropyl (S)-2-tert-butoxycarbonylamino-3-phenylpropanoate

Guidance literature:: With 2-methoxy-phenol; bis(1,5-cyclooctadiene)rhodium(I) hexafluorophosphate; In toluene; at 110 - 115 ℃; for 20h; Title compound not separated from byproducts.;
DOI:10.1021/ja710691p

Reference yield:

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 67-63-0,8013-70-5
isopropyl alcohol

: 247178-99-0
isopropyl (S)-2-tert-butoxycarbonylamino-3-phenylpropanoate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/acs.joc.5b00403