(((2S,3R)-3-(2-bromo-1-ethoxyethoxy)-2-methylpent-4-enyloxy)methyl)benzene

Base Information

Chemical Name:(((2S,3R)-3-(2-bromo-1-ethoxyethoxy)-2-methylpent-4-enyloxy)methyl)benzene
CAS No.:1309924-60-4
Molecular Formula:C₁₇H₂₅BrO₃
Molecular Weight:357.288
Hs Code.:

Synonyms:(((2S,3R)-3-(2-bromo-1-ethoxyethoxy)-2-methylpent-4-enyloxy)methyl)benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (((2S,3R)-3-(2-bromo-1-ethoxyethoxy)-2-methylpent-4-enyloxy)methyl)benzene

Chemical Property:

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Technology Process of (((2S,3R)-3-(2-bromo-1-ethoxyethoxy)-2-methylpent-4-enyloxy)methyl)benzene

There total 4 articles about (((2S,3R)-3-(2-bromo-1-ethoxyethoxy)-2-methylpent-4-enyloxy)methyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2983-26-8
1,2-dibromoethyl ethyl ether

: 96720-54-6
(3R,4S)-5-(benzyloxy)-3-hydroxy-4-methyl-1-pentene

: 1309924-60-4
(((2S,3R)-3-(2-bromo-1-ethoxyethoxy)-2-methylpent-4-enyloxy)methyl)benzene

Guidance literature:: With triethylamine; In dichloromethane; at 25 ℃; Inert atmosphere;
DOI:10.1039/c1ob05240c

Reference yield:

: 79027-28-4
(2S)-3-(benzyloxy)-2-methylpropanal

: 1309924-60-4
(((2S,3R)-3-(2-bromo-1-ethoxyethoxy)-2-methylpent-4-enyloxy)methyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran; diethyl ether / -80 °C / Inert atmosphere

2: triethylamine / dichloromethane / 25 °C / Inert atmosphere

With triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1039/c1ob05240c

Reference yield:

: 74924-27-9
methyl (S)-3-benzyloxy-2-methylpropanoate

: 1309924-60-4
(((2S,3R)-3-(2-bromo-1-ethoxyethoxy)-2-methylpent-4-enyloxy)methyl)benzene

Guidance literature:: Multi-step reaction with 3 steps

1: diisobutylaluminium hydride / diethyl ether; toluene / 0.3 h / -110 °C / Inert atmosphere

2: tetrahydrofuran; diethyl ether / -80 °C / Inert atmosphere

3: triethylamine / dichloromethane / 25 °C / Inert atmosphere

With diisobutylaluminium hydride; triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane; toluene;
DOI:10.1039/c1ob05240c