(3R,4S)-5-(benzyloxy)-3-hydroxy-4-methyl-1-pentene

Base Information

Chemical Name:(3R,4S)-5-(benzyloxy)-3-hydroxy-4-methyl-1-pentene
CAS No.:96720-54-6
Molecular Formula:C₁₃H₁₈O₂
Molecular Weight:206.285
Hs Code.:

Synonyms:(3R,4S)-5-(benzyloxy)-3-hydroxy-4-methyl-1-pentene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3R,4S)-5-(benzyloxy)-3-hydroxy-4-methyl-1-pentene

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Technology Process of (3R,4S)-5-(benzyloxy)-3-hydroxy-4-methyl-1-pentene

There total 7 articles about (3R,4S)-5-(benzyloxy)-3-hydroxy-4-methyl-1-pentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 329366-66-7
(2S)-1-benzyloxy-2-methyl-4-penten-3-one

: 96720-54-6
(3R,4S)-5-(benzyloxy)-3-hydroxy-4-methyl-1-pentene

: 107093-42-5
(3S,4S)-4-methyl-5-(phenylmethoxy)-1-penten-3-ol

Guidance literature:: With zinc borohydride; In diethyl ether; dichloromethane; at -78 - 0 ℃; for 2.5h; stereoselective reaction; Inert atmosphere;
DOI:10.3987/COM-12-12597

Reference yield:

: 882980-43-0
2-benzyloxy-1-methylpyridinium triflate

: 96720-54-6
(3R,4S)-5-(benzyloxy)-3-hydroxy-4-methyl-1-pentene

Guidance literature:: Multi-step reaction with 3 steps

1: magnesium oxide / 1,2-dichloro-ethane / 15 h / Reflux; Inert atmosphere

2: diisobutylaluminium hydride / diethyl ether; toluene / 0.3 h / -110 °C / Inert atmosphere

3: tetrahydrofuran; diethyl ether / -80 °C / Inert atmosphere

With magnesium oxide; diisobutylaluminium hydride; In tetrahydrofuran; diethyl ether; 1,2-dichloro-ethane; toluene;
DOI:10.1039/c1ob05240c