1-benzyl 4-methyl 5-[3-(tert-butyloxycarbonylamino)propanoyl]amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)propanoyl]aminoterephthalate

Base Information

Chemical Name:1-benzyl 4-methyl 5-[3-(tert-butyloxycarbonylamino)propanoyl]amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)propanoyl]aminoterephthalate
CAS No.:1146730-38-2
Molecular Formula:C₄₂H₄₄N₄O₁₀
Molecular Weight:764.832
Hs Code.:

1-benzyl 4-methyl 5-[3-(tert-butyloxycarbonylamino)propanoyl]amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)propanoyl]aminoterephthalate

Synonyms:1-benzyl 4-methyl 5-[3-(tert-butyloxycarbonylamino)propanoyl]amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)propanoyl]aminoterephthalate

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Chemical Property of 1-benzyl 4-methyl 5-[3-(tert-butyloxycarbonylamino)propanoyl]amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)propanoyl]aminoterephthalate

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Technology Process of 1-benzyl 4-methyl 5-[3-(tert-butyloxycarbonylamino)propanoyl]amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)propanoyl]aminoterephthalate

There total 1 articles about 1-benzyl 4-methyl 5-[3-(tert-butyloxycarbonylamino)propanoyl]amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)propanoyl]aminoterephthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 3303-84-2
3-(tert-butyloxycarbonylamino)propionic acid

: 1146730-36-0
1-benzyl 4-methyl 5-amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)-propanoylamino]terephthalate

: 1146730-38-2
1-benzyl 4-methyl 5-[3-(tert-butyloxycarbonylamino)propanoyl]amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)propanoyl]aminoterephthalate

Guidance literature:: 1-benzyl 4-methyl 5-amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)-propanoylamino]terephthalate; With dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 0.0166667h;

With benzotriazol-1-ol; In dichloromethane; at 20 ℃; for 0.0166667h;

3-(tert-butyloxycarbonylamino)propionic acid; In dichloromethane; at 80 ℃; for 48h;
DOI:10.1002/chem.200802151

Reference yield:

: 1146730-38-2
1-benzyl 4-methyl 5-[3-(tert-butyloxycarbonylamino)propanoyl]amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)propanoyl]aminoterephthalate

: 1146730-40-6
5-[3-(tert-butyloxycarbonylamino)propanoyl]amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)propanoyl]aminoterephthalic acid 4-methyl ester

Guidance literature:: With 5%-palladium/activated carbon; hydrogen; In ethyl acetate; at 23 ℃; for 16h; under 760.051 Torr;
DOI:10.1002/chem.200802151