5-[3-(tert-butyloxycarbonylamino)propanoyl]amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)propanoyl]aminoterephthalic acid 4-methyl ester

Base Information

Chemical Name:5-[3-(tert-butyloxycarbonylamino)propanoyl]amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)propanoyl]aminoterephthalic acid 4-methyl ester
CAS No.:1146730-40-6
Molecular Formula:C₃₅H₃₈N₄O₁₀
Molecular Weight:674.708
Hs Code.:

5-[3-(tert-butyloxycarbonylamino)propanoyl]amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)propanoyl]aminoterephthalic acid 4-methyl ester

Synonyms:5-[3-(tert-butyloxycarbonylamino)propanoyl]amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)propanoyl]aminoterephthalic acid 4-methyl ester

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Chemical Property of 5-[3-(tert-butyloxycarbonylamino)propanoyl]amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)propanoyl]aminoterephthalic acid 4-methyl ester

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Technology Process of 5-[3-(tert-butyloxycarbonylamino)propanoyl]amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)propanoyl]aminoterephthalic acid 4-methyl ester

There total 1 articles about 5-[3-(tert-butyloxycarbonylamino)propanoyl]amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)propanoyl]aminoterephthalic acid 4-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1146730-38-2
1-benzyl 4-methyl 5-[3-(tert-butyloxycarbonylamino)propanoyl]amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)propanoyl]aminoterephthalate

: 1146730-40-6
5-[3-(tert-butyloxycarbonylamino)propanoyl]amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)propanoyl]aminoterephthalic acid 4-methyl ester

Guidance literature:: With 5%-palladium/activated carbon; hydrogen; In ethyl acetate; at 23 ℃; for 16h; under 760.051 Torr;
DOI:10.1002/chem.200802151

Reference yield: 94.0%

: 1146730-40-6
5-[3-(tert-butyloxycarbonylamino)propanoyl]amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)propanoyl]aminoterephthalic acid 4-methyl ester

: 58620-93-2
tert-butyl 3-aminopropanoate hydrochloride

: 1146730-42-8
5-[3-(tert-butyloxycarbonylamino)propanoyl]amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)propanoyl]aminoterephthalic acid 1-[2-(tert-butyloxycarbonyl)ethyl]amide 4-methyl ester

Guidance literature:: 5-[3-(tert-butyloxycarbonylamino)propanoyl]amino-2-[3-(fluoren-9-ylmethyloxycarbonylamino)propanoyl]aminoterephthalic acid 4-methyl ester; With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 0.0166667h;

tert-butyl 3-aminopropanoate hydrochloride; With benzotriazol-1-ol; triethylamine; In dichloromethane; at 80 ℃; for 48h;
DOI:10.1002/chem.200802151