7-chloro-3-(2,4-dichlorophenyl)-1,2,3,4,9,10-hexahydroacridine-1,9-dione

Base Information

Chemical Name:7-chloro-3-(2,4-dichlorophenyl)-1,2,3,4,9,10-hexahydroacridine-1,9-dione
CAS No.:91700-87-7
Molecular Formula:C₁₉H₁₂Cl₃NO₂
Molecular Weight:392.669
Hs Code.:

Synonyms:7-chloro-3-(2,4-dichlorophenyl)-1,2,3,4,9,10-hexahydroacridine-1,9-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-chloro-3-(2,4-dichlorophenyl)-1,2,3,4,9,10-hexahydroacridine-1,9-dione

Chemical Property:

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Technology Process of 7-chloro-3-(2,4-dichlorophenyl)-1,2,3,4,9,10-hexahydroacridine-1,9-dione

There total 9 articles about 7-chloro-3-(2,4-dichlorophenyl)-1,2,3,4,9,10-hexahydroacridine-1,9-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 2-(6-Chloro-4-oxo-1,4-dihydro-quinolin-2-yl)-3-(2,4-dichloro-phenyl)-pentanedioic acid diethyl ester

: 91700-87-7
7-chloro-3-(2,4-dichlorophenyl)-1,2,3,4,9,10-hexahydroacridine-1,9-dione

Guidance literature:: With PPA; at 110 - 120 ℃; for 24h;
DOI:10.1080/00397919708004810

Reference yield:

: 66896-92-2,61888-78-6
4-(2',4'-dichlorophenyl)-3-buten-2-one

: 91700-87-7
7-chloro-3-(2,4-dichlorophenyl)-1,2,3,4,9,10-hexahydroacridine-1,9-dione

Guidance literature:: Multi-step reaction with 4 steps

1: EtONa / ethanol / 6 h / Heating

2: 2 N NaOH / 2 h / Heating

3: 5 N H₂SO₄ / 4.5 h / Heating

4: 1.) 50percent NaH / 1.) DMF, RT, 1 h, 2.) DMF, 90 deg C, 4 h

With sodium hydroxide; sulfuric acid; sodium ethanolate; sodium hydride; In ethanol;
DOI:10.1021/jm00097a001

Reference yield:

: 874-42-0
2,4-dichlorobenzaldeyhde

: 91700-87-7
7-chloro-3-(2,4-dichlorophenyl)-1,2,3,4,9,10-hexahydroacridine-1,9-dione

Guidance literature:: Multi-step reaction with 5 steps

1: 78 percent / 50percent aq. NaOH / 72 h / Ambient temperature

2: EtONa / ethanol / 6 h / Heating

3: 2 N NaOH / 2 h / Heating

4: 5 N H₂SO₄ / 4.5 h / Heating

5: 1.) 50percent NaH / 1.) DMF, RT, 1 h, 2.) DMF, 90 deg C, 4 h

With sodium hydroxide; sulfuric acid; sodium ethanolate; sodium hydride; In ethanol;
DOI:10.1021/jm00097a001