((((ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy))bis(5-methoxy-2-nitro-4,1-phenylene))bis(ethane-1,1-diyl)bis(2-methylacrylate)

Base Information

Chemical Name:((((ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy))bis(5-methoxy-2-nitro-4,1-phenylene))bis(ethane-1,1-diyl)bis(2-methylacrylate)
CAS No.:1620973-23-0
Molecular Formula:C₃₂H₄₀N₂O₁₄
Molecular Weight:676.675
Hs Code.:

Synonyms:((((ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy))bis(5-methoxy-2-nitro-4,1-phenylene))bis(ethane-1,1-diyl)bis(2-methylacrylate)

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Chemical Property of ((((ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy))bis(5-methoxy-2-nitro-4,1-phenylene))bis(ethane-1,1-diyl)bis(2-methylacrylate)

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Technology Process of ((((ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy))bis(5-methoxy-2-nitro-4,1-phenylene))bis(ethane-1,1-diyl)bis(2-methylacrylate)

There total 5 articles about ((((ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy))bis(5-methoxy-2-nitro-4,1-phenylene))bis(ethane-1,1-diyl)bis(2-methylacrylate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1620973-22-9
1,1'-((((ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy))bis(5-methoxy-2-nitro-4,1-phenylene))diethanol

: 920-46-7,26937-45-1
Methacryloyl chloride

: 1620973-23-0
((((ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy))bis(5-methoxy-2-nitro-4,1-phenylene))bis(ethane-1,1-diyl)bis(2-methylacrylate)

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 12h; Cooling with ice;
DOI:10.1002/pola.27165

Reference yield:

: 112-26-5,27252-69-3
1,2-bis(2-chloroethoxy)ethane

: 1620973-23-0
((((ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy))bis(5-methoxy-2-nitro-4,1-phenylene))bis(ethane-1,1-diyl)bis(2-methylacrylate)

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 120 °C / Inert atmosphere

2: acetic anhydride; nitric acid / 2 h / 0 - 20 °C

3: sodium tetrahydroborate / tetrahydrofuran / 3 h / 20 °C

4: triethylamine / dichloromethane / 12 h / 20 °C / Cooling with ice

With sodium tetrahydroborate; nitric acid; acetic anhydride; potassium carbonate; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/pola.27165

Reference yield:

: 1620973-19-4
1,1'-((((ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy))bis(3-methoxy-4,1-phenylene))diethanone

: 1620973-23-0
((((ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy))bis(5-methoxy-2-nitro-4,1-phenylene))bis(ethane-1,1-diyl)bis(2-methylacrylate)

Guidance literature:: Multi-step reaction with 3 steps

1: acetic anhydride; nitric acid / 2 h / 0 - 20 °C

2: sodium tetrahydroborate / tetrahydrofuran / 3 h / 20 °C

3: triethylamine / dichloromethane / 12 h / 20 °C / Cooling with ice

With sodium tetrahydroborate; nitric acid; acetic anhydride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1002/pola.27165