O-methyl styelsamine-N¹⁴-3-phenylpropanamide

Base Information

Chemical Name:O-methyl styelsamine-N¹⁴-3-phenylpropanamide
CAS No.:1430088-78-0
Molecular Formula:C₂₇H₂₅N₃O₂
Molecular Weight:423.514
Hs Code.:

O-methyl styelsamine-N<SUP>14</SUP>-3-phenylpropanamide

Synonyms:O-methyl styelsamine-N¹⁴-3-phenylpropanamide

Suppliers and Price of O-methyl styelsamine-N¹⁴-3-phenylpropanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-methyl styelsamine-N¹⁴-3-phenylpropanamide

Chemical Property:

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Technology Process of O-methyl styelsamine-N¹⁴-3-phenylpropanamide

There total 8 articles about O-methyl styelsamine-N¹⁴-3-phenylpropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 1430088-73-5
O-methyl styelsamine D

: 645-45-4
hydrocinnamic acid chloride

: 1430088-78-0
O-methyl styelsamine-N¹⁴-3-phenylpropanamide

Guidance literature:: With PyBOP; triethylamine; In tetrahydrofuran; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.3390/md11020274

Reference yield:

: 2878-60-6
N-(3,4-dimethoxyphenethyl)-3-phenylpropanamide

: 1430088-78-0
O-methyl styelsamine-N¹⁴-3-phenylpropanamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: cerium(III) chloride heptahydrate; silver(l) oxide / acetic acid; methanol / 1.5 h / 40 °C / Inert atmosphere

1.2: 0.5 h / 90 °C

2.1: hydrogenchloride / water / 48 h / 80 °C

3.1: triethylamine; PyBOP / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

With hydrogenchloride; cerium(III) chloride heptahydrate; PyBOP; triethylamine; silver(l) oxide; In tetrahydrofuran; methanol; water; acetic acid;
DOI:10.3390/md11020274

Reference yield:

: 61-54-1
tryptamine

: 1430088-78-0
O-methyl styelsamine-N¹⁴-3-phenylpropanamide

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydroxide / water; ethyl acetate / 0.5 h / 20 °C / Inert atmosphere

2.1: ozone / Cooling with ice

2.2: 1.5 h / 40 °C

3.1: hydrogen bromide / acetic acid / 18 h / 80 °C / Inert atmosphere

4.1: cerium(III) chloride heptahydrate; silver(l) oxide / acetic acid; methanol / 1.5 h / 40 °C / Inert atmosphere

4.2: 0.5 h / 90 °C

5.1: hydrogenchloride / water / 48 h / 80 °C

6.1: triethylamine; PyBOP / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

With hydrogenchloride; cerium(III) chloride heptahydrate; PyBOP; hydrogen bromide; ozone; triethylamine; sodium hydroxide; silver(l) oxide; In tetrahydrofuran; methanol; water; acetic acid; ethyl acetate;
DOI:10.3390/md11020274