C₅₀H₆₅N₃O₂₁Si

Base Information

Chemical Name:C₅₀H₆₅N₃O₂₁Si
CAS No.:1333414-23-5
Molecular Formula:C₅₀H₆₅N₃O₂₁Si
Molecular Weight:1072.16
Hs Code.:

C<sub>50</sub>H<sub>65</sub>N<sub>3</sub>O<sub>21</sub>Si

Synonyms:C₅₀H₆₅N₃O₂₁Si

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Chemical Property of C₅₀H₆₅N₃O₂₁Si

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Technology Process of C₅₀H₆₅N₃O₂₁Si

There total 12 articles about C₅₀H₆₅N₃O₂₁Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 1333414-20-2
C₃₀H₄₆N₂O₁₂Si

: 87190-67-8
3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl-O-trichloroacetimidate

: 1333414-23-5
C₅₀H₆₅N₃O₂₁Si

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 - 20 ℃; for 14h; Inert atmosphere; Molecular sieve;
DOI:10.1021/ol2021687

Reference yield:

: C₂₆H₃₅O₁₁N

: 1333414-23-5
C₅₀H₆₅N₃O₂₁Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: methanol; sodium methylate / 12 h / 20 °C / Inert atmosphere

2.1: toluene-4-sulfonic acid / acetonitrile / 3 h / 20 °C

3.1: sodium hydride / 1,4-dioxane / 60 °C / Inert atmosphere

4.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 2 h / 20 °C / Inert atmosphere

5.1: methanol; toluene-4-sulfonic acid / 1 h / 70 °C

5.2: 20 °C

6.1: dichloromethane / 0.42 h / -78 °C / Inert atmosphere

7.1: pyridine / dichloromethane / 0.83 h / -78 °C / Inert atmosphere

8.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 14 h / -78 - 20 °C / Inert atmosphere; Molecular sieve

With pyridine; methanol; dmap; trimethylsilyl trifluoromethanesulfonate; sodium methylate; sodium hydride; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1,4-dioxane; dichloromethane; acetonitrile;
DOI:10.1021/ol2021687

Reference yield:

: C₁₈H₂₇NO₇

: 1333414-23-5
C₅₀H₆₅N₃O₂₁Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: toluene-4-sulfonic acid / acetonitrile / 3 h / 20 °C

2.1: sodium hydride / 1,4-dioxane / 60 °C / Inert atmosphere

3.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 2 h / 20 °C / Inert atmosphere

4.1: methanol; toluene-4-sulfonic acid / 1 h / 70 °C

4.2: 20 °C

5.1: dichloromethane / 0.42 h / -78 °C / Inert atmosphere

6.1: pyridine / dichloromethane / 0.83 h / -78 °C / Inert atmosphere

7.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 14 h / -78 - 20 °C / Inert atmosphere; Molecular sieve

With pyridine; methanol; dmap; trimethylsilyl trifluoromethanesulfonate; sodium hydride; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1,4-dioxane; dichloromethane; acetonitrile;
DOI:10.1021/ol2021687