N-(6-cyano-1-tosyl-1,2-dihydroquinolin-4-yl)-4-methyl-N-phenylbenzenesulfonamide

Base Information

Chemical Name:N-(6-cyano-1-tosyl-1,2-dihydroquinolin-4-yl)-4-methyl-N-phenylbenzenesulfonamide
CAS No.:1418756-22-5
Molecular Formula:C₃₀H₂₅N₃O₄S₂
Molecular Weight:555.678
Hs Code.:

Synonyms:N-(6-cyano-1-tosyl-1,2-dihydroquinolin-4-yl)-4-methyl-N-phenylbenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(6-cyano-1-tosyl-1,2-dihydroquinolin-4-yl)-4-methyl-N-phenylbenzenesulfonamide

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Technology Process of N-(6-cyano-1-tosyl-1,2-dihydroquinolin-4-yl)-4-methyl-N-phenylbenzenesulfonamide

There total 3 articles about N-(6-cyano-1-tosyl-1,2-dihydroquinolin-4-yl)-4-methyl-N-phenylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1418756-64-5
C₃₀H₂₅N₃O₄S₂

: 1418756-22-5
N-(6-cyano-1-tosyl-1,2-dihydroquinolin-4-yl)-4-methyl-N-phenylbenzenesulfonamide

Guidance literature:: With iron(III) chloride; silver trifluoromethanesulfonate; In 1,2-dichloro-ethane; at 25 - 80 ℃; for 1h; Inert atmosphere;
DOI:10.1002/ejoc.201201270

Reference yield:

: 56768-53-7
N-(4-cyanophenyl)-4-methylbenzenesulfonamide

: 1418756-22-5
N-(6-cyano-1-tosyl-1,2-dihydroquinolin-4-yl)-4-methyl-N-phenylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride

2: copper dichloride; sodium carbonate; pyridine; oxygen

3: iron(III) chloride; silver trifluoromethanesulfonate / 1,2-dichloro-ethane / 1 h / 25 - 80 °C / Inert atmosphere

With pyridine; iron(III) chloride; oxygen; silver trifluoromethanesulfonate; sodium hydride; sodium carbonate; copper dichloride; In 1,2-dichloro-ethane;
DOI:10.1002/ejoc.201201270

Reference yield:

: 68-34-8
phenyl toluenesulfonamide

: 1198272-73-9
C₁₇H₁₄N₂O₂S

: 1418756-22-5
N-(6-cyano-1-tosyl-1,2-dihydroquinolin-4-yl)-4-methyl-N-phenylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: copper dichloride; sodium carbonate; pyridine; oxygen

2: iron(III) chloride; silver trifluoromethanesulfonate / 1,2-dichloro-ethane / 1 h / 25 - 80 °C / Inert atmosphere

With pyridine; iron(III) chloride; oxygen; silver trifluoromethanesulfonate; sodium carbonate; copper dichloride; In 1,2-dichloro-ethane;
DOI:10.1002/ejoc.201201270