6-(4-methoxyphenyl)-3-hexenyl bromide

Base Information

• Chemical Name: 6-(4-methoxyphenyl)-3-hexenyl bromide
• CAS No.: 52121-86-5
• Molecular Formula: C₁₃H₁₇BrO
• Molecular Weight: 269.181
• Mol file: 52121-86-5.mol

Synonyms:6-(4-methoxyphenyl)-3-hexenyl bromide

Chemical Property of 6-(4-methoxyphenyl)-3-hexenyl bromide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 6-(4-methoxyphenyl)-3-hexenyl bromide

There total 6 articles about 6-(4-methoxyphenyl)-3-hexenyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(3-Bromo-3-cyclopropyl-propyl)-4-methoxy-benzene (87141-67-1) → 6-(4-methoxyphenyl)-3-hexenyl bromide (52121-86-5)

Guidance literature:

With zinc dibromide; In diethyl ether; for 1.5h;

Reference yield:

2-(4-Methoxyphenyl)ethyl cyclopropyl carbinol (52121-66-1) → 6-(4-methoxyphenyl)-3-hexenyl bromide (52121-86-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 3.2 g / LiBr, PBr₃, collidine / diethyl ether / 1.5 h / 0 °C

2: 2.8 g / ZnBr₂ / diethyl ether / 1.5 h

With 2,3,5-trimethyl-pyridine; phosphorus tribromide; lithium bromide; zinc dibromide; In diethyl ether;

Reference yield:

1-Cyclopropyl-3-(4-methoxy-phenyl)-propan-1-one (87141-66-0) → 6-(4-methoxyphenyl)-3-hexenyl bromide (52121-86-5)

Guidance literature:

Multi-step reaction with 3 steps

1: 2.98 g / NaBH₄ / methanol / 1.5 h / 0 °C

2: 3.2 g / LiBr, PBr₃, collidine / diethyl ether / 1.5 h / 0 °C

3: 2.8 g / ZnBr₂ / diethyl ether / 1.5 h

With 2,3,5-trimethyl-pyridine; sodium tetrahydroborate; phosphorus tribromide; lithium bromide; zinc dibromide; In methanol; diethyl ether;

upstream raw materials:

1-(3-Bromo-3-cyclopropyl-propyl)-4-methoxy-benzene

2-(4-Methoxyphenyl)ethyl cyclopropyl carbinol

1-Cyclopropyl-3-(4-methoxy-phenyl)-propan-1-one

p-methoxybenzyl chloride

Downstream raw materials:

2-[(E)-6-(4-Methoxy-phenyl)-hex-3-enyl]-3-methyl-cyclohex-2-enone

2-[(E)-6-(4-Methoxy-phenyl)-hex-3-enyl]-1,3-dimethyl-cyclohex-2-enol

1-[(E)-6-(4-Methoxy-phenyl)-hex-3-enyl]-6-methyl-7-oxa-bicyclo[4.1.0]heptan-2-one

6-(4-methoxyphenyl)-hexyl bromide