p-(2-methoxycarbonylethyl)phenyl 2,3,4-tri-O-acethyl-α-L-rhamnopyranoside

Base Information

Chemical Name:p-(2-methoxycarbonylethyl)phenyl 2,3,4-tri-O-acethyl-α-L-rhamnopyranoside
CAS No.:99705-75-6
Molecular Formula:C₂₂H₂₈O₁₀
Molecular Weight:452.458
Hs Code.:

Synonyms:p-(2-methoxycarbonylethyl)phenyl 2,3,4-tri-O-acethyl-α-L-rhamnopyranoside

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Chemical Property of p-(2-methoxycarbonylethyl)phenyl 2,3,4-tri-O-acethyl-α-L-rhamnopyranoside

Chemical Property:

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Technology Process of p-(2-methoxycarbonylethyl)phenyl 2,3,4-tri-O-acethyl-α-L-rhamnopyranoside

There total 1 articles about p-(2-methoxycarbonylethyl)phenyl 2,3,4-tri-O-acethyl-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5597-50-2
3-(4-hydroxyphenyl)propionic acid methyl ester

: 69980-52-5
2,3,4-tri-O-acetyl-L-rhamnopyranosyl bromide

: p-(2-methoxycarbonylethyl)phenyl 2,3,4-tri-O-acethyl-β-L-rhamnopyranoside

: 99705-75-6
p-(2-methoxycarbonylethyl)phenyl 2,3,4-tri-O-acethyl-α-L-rhamnopyranoside

Guidance literature:: With mercury(II) cyanide; In acetonitrile; Yield given; Ambient temperature;

Reference yield:

: 99705-75-6
p-(2-methoxycarbonylethyl)phenyl 2,3,4-tri-O-acethyl-α-L-rhamnopyranoside

: 99694-46-9
p-(2-methoxycarbonylethyl)phenyl 4-O-(2,4-di-O-acetyl-3-O-methyl-β-D-glucopyranosyl)-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 1) sodium methoxide / 1) methanol; 2) acetone, 5h

2: mercury cyanide / acetonitrile / Ambient temperature

4: acetic acid, water / methanol / 0.17 h / Heating

With water; sodium methylate; mercury(II) cyanide; acetic acid; In methanol; acetonitrile;

Reference yield:

: 99705-75-6
p-(2-methoxycarbonylethyl)phenyl 2,3,4-tri-O-acethyl-α-L-rhamnopyranoside

: p-(2-methoxycarbonylethyl)phenyl 4-O-(3,6-di-O-methyl-β-D-glucopyranosyl)-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 7 steps

1: 1) sodium methoxide / 1) methanol; 2) acetone, 5h

2: mercury cyanide / acetonitrile / Ambient temperature

4: acetic acid, water / methanol / 0.17 h / Heating

5: boron trifluoride-etherate / CH₂Cl₂ / 1.5 h / 0 °C

6: acetic acid, water / 0.83 h / Heating

7: sodium methoxide / methanol / 0.03 h / Heating

With boron trifluoride diethyl etherate; water; sodium methylate; mercury(II) cyanide; acetic acid; In methanol; dichloromethane; acetonitrile;