3'-O-(thiocarbonylimidazolyl)-5'-O-benzoyl-5-methyl-2,2'-anhydrouridine

Base Information

Chemical Name:3'-O-(thiocarbonylimidazolyl)-5'-O-benzoyl-5-methyl-2,2'-anhydrouridine
CAS No.:126543-52-0
Molecular Formula:C₂₁H₁₈N₄O₆S
Molecular Weight:454.463
Hs Code.:

Synonyms:3'-O-(thiocarbonylimidazolyl)-5'-O-benzoyl-5-methyl-2,2'-anhydrouridine

Suppliers and Price of 3'-O-(thiocarbonylimidazolyl)-5'-O-benzoyl-5-methyl-2,2'-anhydrouridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 3'-O-(thiocarbonylimidazolyl)-5'-O-benzoyl-5-methyl-2,2'-anhydrouridine

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 3'-O-(thiocarbonylimidazolyl)-5'-O-benzoyl-5-methyl-2,2'-anhydrouridine

There total 2 articles about 3'-O-(thiocarbonylimidazolyl)-5'-O-benzoyl-5-methyl-2,2'-anhydrouridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 126578-22-1
5'-O-benzoyl-5-methyl-2,2'-anhydrouridine

: 6160-65-2
1,1'-Thiocarbonyldiimidazole

: 126543-52-0
3'-O-(thiocarbonylimidazolyl)-5'-O-benzoyl-5-methyl-2,2'-anhydrouridine

Guidance literature:: In N,N-dimethyl-formamide; for 1h;
DOI:10.1021/jm00168a020

Reference yield:

: 120649-55-0
1-(5-O-benzoyl-β-D-ribofuranosyl)thymine

: 126543-52-0
3'-O-(thiocarbonylimidazolyl)-5'-O-benzoyl-5-methyl-2,2'-anhydrouridine

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / diphenyl carbonate, sodium bicarbonate / dimethylformamide / 0.75 h / 120 °C

2: 66 percent / dimethylformamide / 1 h

With bis(phenyl) carbonate; sodium hydrogencarbonate; In N,N-dimethyl-formamide;
DOI:10.1021/jm00168a020

Reference yield: 47.0%

: 126543-52-0
3'-O-(thiocarbonylimidazolyl)-5'-O-benzoyl-5-methyl-2,2'-anhydrouridine

: 126543-53-1
3'-deoxy-5'-O-benzoyl-5-methyl-2,2'-anhydrouridine

Guidance literature:: With azobisisobutyronitrile; tri-n-butyl-tin hydride; In toluene; acetonitrile; for 1h; Heating;
DOI:10.1021/jm00168a020