(E)-2-[Methyl-(2-nitro-benzyl)-amino]-but-2-enedioic acid dimethyl ester

Base Information

Chemical Name:(E)-2-[Methyl-(2-nitro-benzyl)-amino]-but-2-enedioic acid dimethyl ester
CAS No.:363138-96-9
Molecular Formula:C₁₄H₁₆N₂O₆
Molecular Weight:308.291
Hs Code.:

Synonyms:(E)-2-[Methyl-(2-nitro-benzyl)-amino]-but-2-enedioic acid dimethyl ester

Suppliers and Price of (E)-2-[Methyl-(2-nitro-benzyl)-amino]-but-2-enedioic acid dimethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (E)-2-[Methyl-(2-nitro-benzyl)-amino]-but-2-enedioic acid dimethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (E)-2-[Methyl-(2-nitro-benzyl)-amino]-but-2-enedioic acid dimethyl ester

There total 3 articles about (E)-2-[Methyl-(2-nitro-benzyl)-amino]-but-2-enedioic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 56222-08-3
(2-nitrobenzyl)methylamine

: 762-42-5
dimethyl acetylenedicarboxylate

: 363138-96-9
(E)-2-[Methyl-(2-nitro-benzyl)-amino]-but-2-enedioic acid dimethyl ester

Guidance literature:: In toluene; at 20 ℃;
DOI:10.1016/S0040-4039(01)00843-7

Reference yield:

: 612-25-9
2-Nitrobenzyl alcohol

: 363138-96-9
(E)-2-[Methyl-(2-nitro-benzyl)-amino]-but-2-enedioic acid dimethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: NEt₃ / tetrahydrofuran / 20 °C

2: H₂O / 20 °C

3: 100 percent / toluene / 20 °C

With triethylamine; In tetrahydrofuran; water; toluene;
DOI:10.1016/S0040-4039(01)00843-7

Reference yield:

: 163915-96-6
(2-nitrophenyl)methyl methanesulfonate

: 363138-96-9
(E)-2-[Methyl-(2-nitro-benzyl)-amino]-but-2-enedioic acid dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂O / 20 °C

2: 100 percent / toluene / 20 °C

In water; toluene;
DOI:10.1016/S0040-4039(01)00843-7